Method for preparing copper barrier layer-seed crystal layer film
A kind of thin film preparation, barrier layer technology
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specific Embodiment 1
[0032] The production process of the copper barrier layer / seed layer film is: degassing => barrier layer deposition => ion sputtering => seed layer deposition => secondary ion sputtering 2.
[0033] First, carry out the degassing process;
[0034] Next, a barrier layer deposition process is performed: first depositing a tantalum nitride film, and then depositing a metal tantalum film. After the tantalum nitride / tantalum double-layer barrier film deposition process is performed, there are impurity layers such as copper oxide and a tantalum nitride / tantalum double-layer barrier layer on the surface of the lower copper metal at the bottom of the through hole in sequence;
[0035] Subsequently, the ion sputtering process step is carried out. By sputtering, the above two layers of substances will be removed at the same time, exposing the underlying metal surface; moreover, ion sputtering will play the role of heavy sputtering technology, which will have a positive effect on the met...
specific Embodiment 2
[0040] The production process of the copper barrier layer / seed layer film is: degassing => barrier layer deposition => ion sputtering => seed layer deposition. Wherein, the process conditions of the ion sputtering process steps are: the power of the upper radio frequency is 300-800W, the power of the lower radio frequency is 200-700W, and the flow rate of argon gas is 20-150 sccm.
[0041] Compared with the specific embodiment 1, the process steps are simplified, and the dual effects of pre-cleaning and optimizing the pore filling coverage of the barrier film can be satisfied.
[0042] The invention adopts simplified barrier layer chamber design and barrier layer deposition process, which reduces the cost; at the same time, it avoids the problem of particle increase caused by the addition of tantalum heavy sputtering coils;
[0043] Using low-cost ion sputtering pre-cleaning technology, through the optimization of the process flow, the equipment and chip manufacturing costs ar...
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