A kind of preparation method of photocatalytic multifunctional fiber material
A fiber material and multi-functional technology, applied in the field of environmental purification materials, can solve the problems of not having great benefits for the health, the decomposition rate of organic matter, and the low rate of bacterial inhibition, so as to improve the photon efficiency, increase the specific surface area, Eliminate the effect
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Embodiment 1
[0030] A method for preparing a photocatalytic multifunctional fiber material, comprising the following steps:
[0031] (1) Take 180 grams of sodium tungstate in a beaker, first add 3400 mL of deionized water to dissolve completely, then add 1200 mL of dilute hydrochloric acid until all yellow precipitates are formed, after standing for 24 hours, wash and filter the precipitate with deionized water for 3 times, Then add 15% dilute ammonia water to the precipitate until the yellow precipitate is completely converted into a transparent colloid;
[0032] (2) Get 40 grams of samarium oxide and 80 grams of europium oxide in a beaker, add enough dilute nitric acid to dissolve completely, then add 50 grams of ethanol and mix well, stir at room temperature for 0.4 hour to obtain a rare earth nitrate mixed solution;
[0033] (3) Add the transparent colloid to the rare earth nitrate mixed solution, then add 850 mL of deionized water, stir at room temperature for 0.8 hours, then add dilu...
Embodiment 2
[0039] A method for preparing a photocatalytic multifunctional fiber material, comprising the following steps:
[0040] (1) Take 240 grams of ammonium metatungstate in a beaker, first add 4500 mL of deionized water to dissolve completely, then add 1500 mL of dilute nitric acid until all yellow precipitates are formed, after standing for 30 hours, wash and filter the precipitate with deionized water for 5 times , and then add 15% dilute ammonia water to the precipitate until the yellow precipitate is completely converted into a transparent colloid;
[0041] (2) Get 160 grams of praseodymium oxide in a beaker, add a sufficient amount of dilute nitric acid to dissolve completely, then add 80 grams of glacial acetic acid and mix uniformly, stir at room temperature for 0.6 hour to obtain a rare earth nitrate mixed solution;
[0042] (3) Add the transparent colloid to the rare earth nitrate mixed solution, then add 1500 mL of deionized water, stir at room temperature for 1.2 hours, th...
Embodiment 3
[0048] A method for preparing a photocatalytic multifunctional fiber material, comprising the following steps:
[0049] (1) Take 210 grams of potassium tungstate in a beaker, first add 4000 mL of deionized water to dissolve completely, then add 1200 mL of dilute sulfuric acid until all yellow precipitates are formed, after standing for 27 hours, wash and filter the precipitate with deionized water for 4 times, Then add 15% dilute ammonia water to the precipitate until the yellow precipitate is completely converted into a transparent colloid;
[0050] (2) Take 40 grams of erbium oxide, 40 grams of neodymium oxide, 40 grams of gadolinium oxide, and 20 grams of cerium oxide in a beaker, add enough dilute nitric acid to dissolve completely, then add 70 grams of methanol and mix well. Stir for 0.5 hour to obtain a rare earth nitrate mixed solution;
[0051] (3) Add the transparent colloid to the rare earth nitrate mixed solution, then add 1200mL of deionized water, stir at room te...
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