A kind of preparation method of photocatalytic multifunctional fiber material

A fiber material and multi-functional technology, applied in the field of environmental purification materials, can solve the problems of not having great benefits for the health, the decomposition rate of organic matter, and the low rate of bacterial inhibition, so as to improve the photon efficiency, increase the specific surface area, Eliminate the effect

Active Publication Date: 2016-03-02
苏州风享环保科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Compared with coatings, floors, glass, ceramics and other materials, photocatalytic multifunctional fiber materials have a larger specific surface area, so they can fully contact with organic pollutants in the air, and can eliminate organic pollution in the air more quickly and efficiently substances, reducing heavy metal inorganic ions, sterilizing and deodorizing, etc., but currently there are very few fiber materials with this function, and the few fiber materials have low organic matter decomposition rate and bacterial inhibition rate, which are harmful to human health. less than great benefit

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] A method for preparing a photocatalytic multifunctional fiber material, comprising the following steps:

[0031] (1) Take 180 grams of sodium tungstate in a beaker, first add 3400 mL of deionized water to dissolve completely, then add 1200 mL of dilute hydrochloric acid until all yellow precipitates are formed, after standing for 24 hours, wash and filter the precipitate with deionized water for 3 times, Then add 15% dilute ammonia water to the precipitate until the yellow precipitate is completely converted into a transparent colloid;

[0032] (2) Get 40 grams of samarium oxide and 80 grams of europium oxide in a beaker, add enough dilute nitric acid to dissolve completely, then add 50 grams of ethanol and mix well, stir at room temperature for 0.4 hour to obtain a rare earth nitrate mixed solution;

[0033] (3) Add the transparent colloid to the rare earth nitrate mixed solution, then add 850 mL of deionized water, stir at room temperature for 0.8 hours, then add dilu...

Embodiment 2

[0039] A method for preparing a photocatalytic multifunctional fiber material, comprising the following steps:

[0040] (1) Take 240 grams of ammonium metatungstate in a beaker, first add 4500 mL of deionized water to dissolve completely, then add 1500 mL of dilute nitric acid until all yellow precipitates are formed, after standing for 30 hours, wash and filter the precipitate with deionized water for 5 times , and then add 15% dilute ammonia water to the precipitate until the yellow precipitate is completely converted into a transparent colloid;

[0041] (2) Get 160 grams of praseodymium oxide in a beaker, add a sufficient amount of dilute nitric acid to dissolve completely, then add 80 grams of glacial acetic acid and mix uniformly, stir at room temperature for 0.6 hour to obtain a rare earth nitrate mixed solution;

[0042] (3) Add the transparent colloid to the rare earth nitrate mixed solution, then add 1500 mL of deionized water, stir at room temperature for 1.2 hours, th...

Embodiment 3

[0048] A method for preparing a photocatalytic multifunctional fiber material, comprising the following steps:

[0049] (1) Take 210 grams of potassium tungstate in a beaker, first add 4000 mL of deionized water to dissolve completely, then add 1200 mL of dilute sulfuric acid until all yellow precipitates are formed, after standing for 27 hours, wash and filter the precipitate with deionized water for 4 times, Then add 15% dilute ammonia water to the precipitate until the yellow precipitate is completely converted into a transparent colloid;

[0050] (2) Take 40 grams of erbium oxide, 40 grams of neodymium oxide, 40 grams of gadolinium oxide, and 20 grams of cerium oxide in a beaker, add enough dilute nitric acid to dissolve completely, then add 70 grams of methanol and mix well. Stir for 0.5 hour to obtain a rare earth nitrate mixed solution;

[0051] (3) Add the transparent colloid to the rare earth nitrate mixed solution, then add 1200mL of deionized water, stir at room te...

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Abstract

The invention relates to a photocatalytic multifunctional fiber material and a preparation method thereof, belonging to the technical field of materials. The invention mainly solves the technical problems that the decomposition rate of organic matters of the exiting fiber materials is low, the sterilizing and bacteriostatic effect is not obvious and the like. The fiber material is formed by polypropylene master batches and polypropylene slices. The preparation method comprises the following steps: converting tungstate into colloid; using rare earth oxide to prepare rare earth nitrate mixed solution; adding the colloid into the rare earth nitrate mixed solution and dripping dilute acid to form sol; adding catalyst promoter material in the sol to obtain wet gel; after drying and sintering the wet gel, conducting ultrasonic dispersion to obtain powder; adding dried polypropylene matrix, dispersing agent, coupling agent and defoaming agent in the powder and preparing polypropylene master batches through a screw extruder; and adding polypropylene slices in the polypropylene master batches and preparing the photocatalytic multifunctional fiber material through the screw extruder, a melt spinning technology and a deformation technology. The invention has the advantages of high organic matter decomposition rate, good sterilizing effect and the like.

Description

technical field [0001] The invention belongs to the technical field of environmental purification materials, and in particular relates to a method for preparing a photocatalytic multifunctional fiber material. Background technique [0002] With the progress of society and the improvement of people's living standards, people have put forward higher requirements for the quality of life. People's purchase of houses, room decoration, and the application and promotion of petroleum, coal, natural gas, chemical products, automobiles, etc., have brought a certain degree of pollution to our indoor and outdoor air while improving our living standards, especially in recent years. Increasingly luxurious, indoor and outdoor air pollution caused by extensive use of household chemicals, smoking, cooking and other human activities can no longer be ignored, and the quality of the environment directly affects people's health. For people's health, people invented photocatalysis Technology, us...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D01F6/46D01F1/10B29C47/92B29C48/92
CPCB29C48/04B29C48/92B29C2948/92704B29C2948/92895
Inventor 田小兵
Owner 苏州风享环保科技有限公司
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