Double colour fluorescent chemical sensor used for visually detecting explosive and manufacturing method thereof
A dual emission fluorescence, chemical sensor technology, applied in fluorescence/phosphorescence, material excitation analysis, etc., to achieve the effect of good selectivity, simple operation and high sensitivity
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[0029] Example 1
[0030] 1. Preparation of silicon oxide nanoparticles with stable luminescence and embedded quantum dots
[0031] 0.2284g cadmium chloride (CdCl 2 ·2.5H 2 O) Add to 250mL of deoxygenated ultrapure water, then add 0.21mL of mercaptopropionic acid, and then adjust the pH to 11.2 with 1M NaOH solution to form a solution containing mercapto compounds and cadmium ions. On the other hand, 0.0319g of tellurium powder and 0.05g of sodium borohydride were put in 2mL of ultrapure water, and under the protection of nitrogen, the reaction was carried out in an ice bath for more than 8 hours. Inject 5 mL of 0.5M dilute sulfuric acid solution into the resulting sodium tellurium hydride solution. Will generate H 2 All Te was passed into the cadmium ion solution, stirred for 20 minutes, and heated to reflux. By controlling the reflux time, an aqueous solution of cadmium telluride quantum dots with stable mercaptopropionic acid and a fluorescence emission peak at 490-680 nm can ...
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[0037] Example 2
[0038] 1. Preparation of silicon oxide nanoparticles with stable luminescence and embedded quantum dots
[0039] 0.2284g cadmium chloride (CdCl 2 ·2.5H 2 O) Add to 250mL of deoxygenated ultrapure water, then add 0.21mL of mercaptopropionic acid, and then adjust the pH to 11.2 with 1M NaOH solution to form a solution containing mercapto compounds and cadmium ions. On the other hand, 0.0319g of tellurium powder and 0.05g of sodium borohydride were put in 2mL of ultrapure water, and under the protection of nitrogen, the reaction was carried out in an ice bath for more than 8 hours. Inject 5 mL of 0.5 M dilute sulfuric acid solution into the resulting sodium tellurium hydride solution. Will generate H 2 All Te was passed into the cadmium ion solution, stirred for 20 minutes, and heated to reflux. By controlling the reflux time, an aqueous solution of cadmium telluride quantum dots with stable mercaptopropionic acid and a fluorescence emission peak at 490-680 nm can...
Example Embodiment
[0045] Example 3
[0046] 1. Preparation of silicon oxide nanoparticles with stable luminescence and embedded quantum dots
[0047] 0.2284g cadmium chloride (CdCl 2 ·2.5H 2 O) Add to 250mL of deoxygenated ultrapure water, then add 0.21mL of mercaptopropionic acid, and then adjust the pH to 11.2 with 1M NaOH solution to form a solution containing mercapto compounds and cadmium ions. On the other hand, 0.0319g of tellurium powder and 0.05g of sodium borohydride were put in 2mL of ultrapure water, and under the protection of nitrogen, the reaction was carried out in an ice bath for more than 8 hours. Inject 5 mL of 0.5M dilute sulfuric acid solution into the resulting sodium tellurium hydride solution. Will generate H 2 All Te was passed into the cadmium ion solution, stirred for 20 minutes, and heated to reflux. By controlling the reflux time, an aqueous solution of cadmium telluride quantum dots with stable mercaptopropionic acid and a fluorescence emission peak at 490-680 nm can ...
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