Technology for preparing mineral composite solid lubricant for well drilling on basis of by-products in chemical industry
A technology of solid lubricants and by-products, which is applied in the field of mineral composite solid lubricants, can solve problems such as environmental pollution by-products of hydrosulfite, high environmental protection treatment operation costs, etc., and achieve excellent comprehensive lubrication performance, which is conducive to clean production and comprehensive performance excellent effect
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Embodiment 1
[0040] The raw materials for preparation are: hydrosulfite by-product residue (or raffinate), surface-modified graphite with a carbon content of 95% under a 100-mesh sieve, flexible expanded graphite with an expansion multiple of 137 times, REO vegetable oil, and a comprehensive performance modifier for drilling fluid (made by Natural asphalt (NA), hydroxyethyl cellulose (HEC), sorbitan monooleate (SPAN) are prefabricated according to the ratio of 3:1:2 by mass percentage).
[0041] The ratio of raw materials is: by mass percentage, 20-50% of hydrosulfite by-product, 10-50% of graphite, 0-20% of expanded graphite, 5-30% of REO vegetable oil, and 10-40% of drilling fluid comprehensive performance regulator. However, the best raw material ratio is 50% of hydrosulfite by-product residue, 15% of surface-modified flake graphite, 5% of flexible expanded graphite, 15% of REO vegetable oil, and 15% of drilling fluid comprehensive performance regulator.
[0042] The preparation method ...
Embodiment 2
[0047] The raw materials for preparation are: hydrosulfite by-product residue (or raffinate), graphite with a carbon content of 90% under a 200-mesh sieve, expanded graphite with an expansion multiple of 150 times, REO animal oil alkanolamide oil-based surfactant, comprehensive performance of drilling fluid Regulator (pre-made from oxidized asphalt (OSA), carboxymethyl cellulose (CMC), cetyltrimethylammonium bromide (CTAB) according to the ratio of 3:2:1 by mass percentage).
[0048] The ratio of raw materials is: by mass percentage, 20-60% of hydrosulfite by-product, 10-60% of graphite and expanded graphite, 5-30% of REO animal oil alkanolamide oil-based surfactant, and 10-60% of drilling fluid comprehensive performance regulator 40%. However, the best raw material ratio is 50% of hydrosulfite by-product residue, 5% of flake graphite, 10% of expanded graphite, 20% of REO animal oil alkanolamide oil-based surfactant, and 15% of drilling fluid comprehensive performance regulato...
Embodiment 3
[0054] The preparation raw materials are: hydrosulfite by-product residue (or raffinate), expanded graphite with an expansion factor of 200 times, REO animal oil, drilling fluid comprehensive performance regulator (composed of sulfonated pitch (FT-342), carboxymethyl starch ether ( CMS), sodium dodecylbenzenesulfonate (ABS) are prefabricated according to the ratio of 3:1:1 by mass percentage).
[0055] The ratio of raw materials is as follows: by mass percentage, 20-60% of hydrosulfite by-product, 10-30% of expanded graphite, 5-30% of REO animal oil, and 10-40% of drilling fluid comprehensive performance regulator. However, the ratio of raw materials is preferably 50% of hydrosulfite by-product, 10% of expanded graphite, 25% of REO animal oil, and 15% of drilling fluid comprehensive performance modifier.
[0056] The preparation method is as follows:
[0057] (1) After mixing and absorbing the hydrosulfite by-product residue, REO animal oil, and expanded graphite, use known m...
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