A kind of preparation method of feed additive-amino acid trace element chelate
A feed additive and trace element technology, applied in the direction of animal feed, animal feed, additional food elements, etc., can solve the problems of poor stability, low biological utilization rate, and unstable composition, and achieve good product quality, easy promotion, and production. low cost effect
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Embodiment 1
[0017] Dilute methionine and ferrous sulfate with 2.5 times of water to prepare an aqueous solution, send the aqueous methionine solution to the chemical reaction kettle, keep the normal temperature, start the agitator, add the aqueous solution of ferrous sulfate in a molar ratio of 2:1, and oxidize it with hydrogen Sodium aqueous solution is used to adjust the pH value so that it is always maintained at about 7.2. React for 0.5 hours. The reactant is sent to a centrifuge for separation to remove water. Add absolute ethanol to the separated solid at a ratio of 1:1, filter off the absolute ethanol for reuse after stirring, and send the remaining ferrous methionine into a dryer to seal and dry, and then crush and pack the dried product to obtain a finished product .
Embodiment 2
[0019] Dilute methionine and copper sulfate with 2.5 times of water to make an aqueous solution, put the aqueous solution of methionine into the chemical reaction kettle, keep the normal temperature, start the stirrer, add the aqueous solution of copper sulfate according to the molar ratio of 2.1:1, and use the aqueous solution of sodium hydroxide Adjust the pH so that it is always around 7. React for 0.5 hours. The reactant is sent to a centrifuge for separation to remove water. The separated solid is added with absolute ethanol at a ratio of 1:1, and after stirring, the absolute ethanol is filtered off for recycling, and the remaining copper methionine is sent to a dryer for sealing and drying, and then the dried matter is crushed and packaged to obtain a finished product.
Embodiment 3
[0021] Dilute methionine and manganese sulfate with 2.5 times of water to make an aqueous solution, put the methionine aqueous solution into the chemical reaction kettle, keep the normal temperature, start the stirrer, add manganese sulfate aqueous solution in a molar ratio of 2.2:1, and use sodium hydroxide aqueous solution Adjust the pH value to keep it around 7.2. React for 0.5 hours. The reactant is sent to a centrifuge for separation to remove water. The separated solid is added with absolute ethanol at a ratio of 1:1, and after stirring, the absolute ethanol is filtered off for recycling, and the remaining manganese methionine is sent to a dryer for sealing and drying, and then the dried matter is crushed and packaged to obtain a finished product.
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