Flame retardant smoke-suppression type humidity controlling functional coating and preparation method thereof
A functional coating and smoke-suppressing technology, which is applied in the coating and other directions, can solve the problems of poor scrub resistance and low strength
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Embodiment 1
[0026] (1) Rinse the purchased hydrotalcite raw material with deionized water and let it stand for 2 hours; dissolve hydrotalcite and sodium methacryl sulfonate in N,N'-dimethylacetamide organic solvent in a mass ratio of 3:2 , and fully stirred for 24h under the condition of heating to 78°C. Afterwards, the reaction solution was taken out, suction filtered, washed, vacuum-dried at 70° C. for 24 hours, ground and pulverized to obtain the organically modified hydrotalcite.
[0027] (2) Prepare a NaOH aqueous solution with a mass fraction of 25%, and slowly drop the metered NaOH solution into acrylic acid under ice-water bath conditions to obtain an acrylic acid-sodium acrylate solution with a neutralization degree of 70%; then press the sum of the mass of acrylic acid and sodium acrylate The mass ratio of acrylamide to acrylamide is 1:1. Add acrylamide into the above solution to prepare a monomer solution. Then, organically modified hydrotalcite with 2% mass of the monomer sol...
Embodiment 2
[0032] (1) Rinse the purchased hydrotalcite raw material with deionized water and let it stand for 2 hours; dissolve hydrotalcite and sodium methacryl sulfonate in N,N'-dimethylacetamide organic solvent in a mass ratio of 3:2 , and fully stirred for 24h under the condition of heating to 78°C. Afterwards, the reaction solution was taken out, suction filtered, washed, vacuum-dried at 70° C. for 24 hours, ground and pulverized to obtain the organically modified hydrotalcite.
[0033] (2) preparation mass fraction is the NaOH aqueous solution of 25%, under ice-water bath condition, metering NaOH solution is slowly dripped in acrylic acid, obtains the acrylic acid-sodium acrylate solution of 80% neutralization degree; Then press the sum of acrylic acid and sodium acrylate and The mass ratio of acrylamide is 5:1. Add acrylamide into the above solution to prepare a monomer solution. Then, organically modified hydrotalcite with 4% mass of the monomer solution was added into the monom...
Embodiment 3
[0037] (1) Rinse the purchased hydrotalcite raw material with deionized water and let it stand for 2 hours; dissolve hydrotalcite and sodium methacryl sulfonate in N,N'-dimethylacetamide organic solvent in a mass ratio of 3:2 , and fully stirred for 24h under the condition of heating to 78°C. Afterwards, the reaction solution was taken out, suction filtered, washed, vacuum-dried at 70° C. for 24 hours, ground and pulverized to obtain the organically modified hydrotalcite.
[0038] (2) preparation mass fraction is the NaOH aqueous solution of 25%, under ice-water bath condition, metering NaOH solution is slowly dripped in acrylic acid, obtains the acrylic acid-sodium acrylate solution of 90% neutralization degree; Then press the sum of acrylic acid and sodium acrylate and Acrylamide was added to the above solution at a mass ratio of 9:1 to prepare a monomer solution. Then, organically modified hydrotalcite with a mass of 8% of the monomer solution was added into the monomer so...
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