Preparation method of polyvinyl alcohol composite film with embedded silver-wrapped nanoparticles
A technology of silver nanoparticles and polyvinyl alcohol, which is applied in the field of composite material preparation of metal nanoparticles prepared by ultraviolet light reduction method, can solve the problems of surface passivation of nanoparticles, deterioration of mechanical properties of polymer matrix, side reactions, etc., and achieve Relieve oxidation and agglomeration, avoid side reactions, uniform size effect
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[0021] The preparation method of polyvinyl alcohol embedded silver nano particle composite film of the present invention comprises the following steps:
[0022] ① Preparation of polyvinyl alcohol-silver nitrate solution:
[0023] Dissolve the polyvinyl alcohol powder in deionized water according to the ratio of 7-9g polyvinyl alcohol powder per 100ml of water, and let it stand for swelling; raise the temperature to 93-98°C under the condition of magnetic stirring, return the condenser tube to evaporate the solvent, and heat Until the solution becomes a uniform transparent viscous shape, it is called a polyvinyl alcohol solution. After the polyvinyl alcohol solution is cooled to room temperature in the ambient air, dilute nitric acid is added dropwise to adjust the pH value of the polyvinyl alcohol solution. The value ranges from 1 to 5.6; silver nitrate aqueous solution is added to the polyvinyl alcohol solution to form a polyvinyl alcohol-silver nitrate solution, wherein the ...
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