Method for detecting ten-flavour rankincense preparation

Abstract

The invention provides a method for detecting a traditional Tibetan medicine, namely a ten-flavour rankincense preparation. The method is used for detecting frankincense, elecampane and semen cassia in the ten-flavour rankincense preparation through a thin-layer chromatography and comprises the following steps of: (1), preparing a frankincense sample solution group, an elecampane sample solution group and a semen cassia sample solution group; and (2), respectively spotting the three groups of samples prepared in the step (1) on three silica gel G thin-layer plates, developing the samples through a developer, spraying a vanillic aldehyde sulfuric acid solution on the samples, air drying the samples till spots are developed clearly, and detecting the samples. The detection method disclosed by the invention carries out detection and research of frankincense, elecampane and semen cassia through the thin-layer chromatography; the improved thin-layer chromatography has the advantages of being good in repeatability and stability, simple and convenient for operation, high in precision, strong in specificity, clear in spot development, good in separation degree and the like; and the quality standard of the ten-flavour rankincense preparation can be effectively controlled by establishing a quality detection method which is reliable in method and strong in specificity, thus, the quality of the ten-flavour rankincense preparation is steady, controllable and safe.

Description

technical field [0001] The invention relates to a detection method of a pharmaceutical composition preparation, in particular to a detection method of a ten-flavor frankincense preparation, which belongs to the technical field of traditional Chinese medicine detection. Background technique [0002] Shiwei frankincense pills are Tibetan medicines, which are recorded in the Tibetan medicine sub-volume of "Drug Standards of the Ministry of Health of the People's Republic of China", and the standard number is WS3-BC-0211-95. [0003] Prescription: 100g frankincense, 150g myrobalan, 80g cassia, 100g myrobalan, 80g emblical, 120g emblical, 85g woody, 100g broad vine, 80g pashaga, 50g slag taming paste. [0004] Preparation method: the above ten flavors, except the slag taming paste, the rest are crushed into fine powder, sieved, mixed, and the slag taming paste is added with appropriate amount of water to form a pill, dried, and obtained. [0005] It is mainly used to treat redne...

AI Technical Summary

Problems solved by technology

[0007] The reproducibility of the identification of frankincense and cassia seeds in the original standard was not good, and the controllability of the detection method of the quality standard of Shiwei frankincense pills could not be realized, so it was modified on the basis of it; the identification method of frankincense in the original ministerial standard was also made Appropriate revisions have been made to the identification method of cassia seeds in order to provide a method with good reproducibility and strong specificity, which conforms to the principles of accuracy, simplicity, sensitivity and speed, and can effectively control the quality of the product.

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