Microwave-assisted method for extracting tea saponin
A microwave-assisted, tea saponin technology, which is applied in chemical instruments and methods, preparation of sugar derivatives, steroids, etc., can solve the problems of high cost, low extraction purity, low efficiency, etc. Extract cycle, light color effect
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[0023] A) Crush the defatted camellia seed meal, pass a 40-mesh sieve, and dry the powder with a particle size of less than 40 mesh; weigh 500g of the camellia seed meal powder and dissolve it in a 50% ethanol solution. The amount of the ethanol solution is 2L;
[0024] B) The solution obtained in step A is subjected to microwave radiation treatment while stirring, the microwave power is 200-400W, the frequency is 2450MHZ, the treatment time is 4min, and the temperature is 45-55°C;
[0025] C) Suction filtration and centrifugation of the solution treated in step B to obtain the tea saponin extract, which is evaporated and concentrated under a vacuum of 0.8 MPa, and then vacuum dried to obtain crude tea saponin;
[0026] D) Weigh 50g of crude tea saponin obtained in step C, prepare 1L of crude tea saponin aqueous solution, add 10ml of 1% alum aqueous solution, stir and flocculate for 1h and then filter;
[0027] E) Add 250ml of calcium hydroxide solution to the filtrate obtained in step...
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