Method for growing high-quality gallium nitride epitaxial film on basis of gallium nitride substrate
A gallium nitride substrate and epitaxial thin film technology, applied in the semiconductor field, can solve the problems affecting the practical progress of GaN-based materials, and achieve the effects of simple and easy method, short growth period and high crystal quality
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Embodiment 1
[0017] Such as figure 1 As shown, a method for growing a high-quality gallium nitride epitaxial film based on a gallium nitride substrate of the present invention is characterized in that it comprises the following steps:
[0018] 1) Select a substrate 1, which is a 0001-plane self-supporting gallium nitride substrate material;
[0019] 2) Put the substrate 1 into the metal organic chemical vapor deposition system, pass H 2 , the reaction chamber pressure is 100torr, and heated at 1050°C for 5min to clean the substrate surface and remove surface contamination;
[0020] 3) The temperature of the reaction chamber is lowered to 1000°C, and high-purity ammonia gas is introduced for nitriding, H 2 as a carrier gas. The reaction chamber pressure is 300torr, and the nitriding time is 3min;
[0021] 4) Reduce the temperature to 1020°C, reduce the pressure of the reaction chamber to 50torr, continue to pass in ammonia gas, and at the same time pass in trimethylgallium, and epitaxia...
Embodiment 2
[0024] Such as figure 1 As shown, a method for growing a high-quality gallium nitride epitaxial film based on a gallium nitride substrate of the present invention is characterized in that it comprises the following steps:
[0025] 1) Select a substrate 1, which is a 0001-plane self-supporting gallium nitride substrate material;
[0026] 2) Put the substrate 1 into the metal organic chemical vapor deposition system, pass H 2 , the reaction chamber pressure is 200torr, and heated at 1100°C for 3min to clean the substrate surface and remove surface contamination;
[0027] 3) The temperature of the reaction chamber is lowered to 1050°C, and high-purity ammonia gas is introduced for nitriding, H 2 as a carrier gas. The reaction chamber pressure is 500torr, and the nitriding time is 1min;
[0028] 4) Reduce the temperature to 980°C, reduce the pressure of the reaction chamber to 100torr, continue to pass in ammonia gas, and at the same time pass in trimethylgallium, and epitaxia...
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