Easily-degradable alkali-free viscosity reducer for thick oil and preparation method thereof
A heavy oil viscosity reducer, easy to degrade technology, applied in the field of heavy oil viscosity reducer, easy to degrade alkali-free heavy oil viscosity reducer, can solve the problems of corrosion, difficult to degrade, unfavorable demulsification and dehydration, etc. Good capacity, fast biodegradation rate, and good compatibility
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Embodiment 1
[0032] This embodiment provides an easily degradable alkali-free heavy oil viscosity reducer, which is prepared according to the following steps:
[0033] Under normal pressure, first add 55g of water into a four-necked flask equipped with an electric heating mantle, start the stirrer, adjust the rotation speed to 60-120 rpm, and raise the temperature at the same time, and the temperature is controlled at about 65°C;
[0034] Then slowly add L6415g, fatty alcohol ammonium sulfate 15g, lauryl alcohol 5g, fatty alcohol polyoxyethylene ether 10g in order, and mix and stir through 60-90 minutes, promptly obtain 100g active ingredient content and be 45wt% (mass percentage) Viscosity reducer.
[0035]Weigh 60g, 70g, 80g of dehydrated extra heavy oil with a viscosity of 12730mPa·s at 50°C, add 40g, 30g, 20g of the aqueous solution containing 0.3% (mass percentage) of the viscosity reducing agent of this embodiment respectively, and stir at 50°C After 1 minute, three parts of emulsif...
Embodiment 2
[0037] This embodiment provides an easily degradable alkali-free heavy oil viscosity reducer, which is prepared according to the following steps:
[0038] Under normal pressure, first add 40g of water into a four-necked flask equipped with an electric heating mantle, start the stirrer, adjust the speed to 60-120 rpm, and raise the temperature at the same time, and control the temperature at about 65°C;
[0039] Then slowly add L6425g, fatty alcohol ammonium sulfate 25g, lauryl alcohol 4g, fatty alcohol polyoxyethylene ether 6g in order, and through mixing and stirring for 60-90 minutes, 100g of active ingredient content is 60wt% (mass percentage) Viscosity reducer, denoted as J-2.
[0040] Weigh 60g, 70g, 80g of dehydrated super heavy oil with a viscosity of 57320mPa·s at 50°C, add 40g, 30g, 20g of the aqueous solution containing 0.3% (mass percentage) of the viscosity reducing agent of this embodiment respectively, and After stirring for 1 minute, three parts of emulsified h...
Embodiment 3
[0045] In this embodiment, the demulsification and dehydration performance test is carried out on the viscosity reducer prepared in Example 2, which specifically includes the following steps:
[0046] Measure four parts of ordinary heavy oil (water content 28wt%) with a viscosity of 2180mPa·s at 50°C and contain bound water, each part is 70mL, numbered I, II, III, IV respectively;
[0047] In I, II, add the viscosity reducer J-2 concentration that embodiment 2 prepares to be the aqueous solution 30mL of 0.3% (mass percentage), in III, IV, add PS viscosity reducer (produced by Huayou Industrial Company of Liaohe Oilfield) 0.3 % (mass percentage) aqueous solution of 30mL, stirred at 50°C for 1 minute, after all the emulsions are formed, then add 2-3 drops of demulsifier P-1 (TR-DEM / LY-IV type) to II and IV respectively Water-soluble crude oil demulsifier, produced by Liaohe Oilfield Huayou Hongshan Chemical Factory), mix and stir evenly, then quickly transfer I, II, III, and IV ...
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