Composite film with photocatalytic function and preparation method thereof
A composite film, photocatalytic technology, applied in the field of photocatalytic materials, can solve the problem of low adsorption index, achieve the effect of large adsorption capacity, easy regeneration, and improve photocatalytic efficiency
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Embodiment 1
[0031] (1) First select industrial pure Ti to process the matrix material for photocatalytic degradation of organic matter;
[0032] (2) Pure titanium pretreatment: use metallographic sandpaper with labels of 600#, 800#, 1000#, and 1200# to polish the pure titanium base material step by step from coarse sand to fine sand, and then use acetone, alcohol, distilled water Ultrasonic cleaning, dry for use.
[0033] (3) Electrolyte configuration: use sodium carbonate solution system, configure 10L sodium carbonate solution with a concentration of 15g / L and potassium hydroxide solution with a concentration of 2g / L, stir and dissolve at a constant temperature of 40°C, and set aside;
[0034] (4) Micro-arc oxidation of pure titanium: place the pure titanium substrate in the electrolytic cell of the bipolar pulse micro-arc oxidation equipment and add the prepared electrolyte, use pure titanium as the anode, and the stainless steel electrolytic cell as the cathode, adjust the process par...
Embodiment 2
[0038] (1) First select the medical Ti6Al4V alloy to process the photodynamic therapy matrix material;
[0039] (2) Titanium alloy pretreatment: The titanium alloy substrate is polished and polished step by step from coarse sand to fine sand using metallographic sandpaper with labels of 600#, 800#, 1000#, and 1200#, and then ultrasonicated with acetone, alcohol, and distilled water Wash, dry and set aside.
[0040] (3) Electrolyte configuration: use sodium carbonate solution system, configure 10L sodium carbonate solution with a concentration of 15g / L and potassium hydroxide solution with a concentration of 2g / L, stir and dissolve at a constant temperature of 40°C, and set aside;
[0041] (4) Micro-arc oxidation of titanium alloy: place the titanium alloy in the electrolytic cell of the bipolar pulse micro-arc oxidation equipment and add the prepared electrolyte, use the Ti6Al4V alloy as the anode, and the stainless steel electrolytic cell as the cathode, adjust the process pa...
Embodiment 3
[0045] (1) First, select industrial Ti6Al4V to process the matrix material for photocatalytic degradation of organic matter;
[0046] (2) Ti6Al4V pretreatment: use metallographic sandpaper with labels of 600#, 800#, 1000#, and 1200# to polish and polish the base material step by step from coarse sand to fine sand, and then ultrasonically clean it with acetone, alcohol, and distilled water. Dry and set aside.
[0047] (3) Electrolyte configuration: use sodium carbonate solution system, configure 10L sodium carbonate solution with a concentration of 15g / L and potassium hydroxide solution with a concentration of 2g / L, stir and dissolve at a constant temperature of 40°C, and set aside;
[0048] (4) Micro-arc oxidation of Ti6Al4V substrate: place the titanium alloy in the electrolytic cell of the bipolar pulse micro-arc oxidation equipment and add the prepared electrolyte, use Ti6Al4V as the anode, and the stainless steel electrolytic cell as the cathode, and adjust the process par...
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