Temperature-resistant thermal-spray radar absorbing coating and preparation method of spraying powder thereof
A technology of wave absorbing coating and spraying powder, applied in the direction of coating, metal material coating process, melting spray plating, etc., can solve the problem of low temperature resistance of wave absorbing coating, and achieve good wave absorbing performance and mechanical performance. Excellent effect with simple preparation process
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[0039] Further, the preparation method of the above-mentioned spray powder for radar absorbing coating of the present invention includes the following steps:
[0040] Step 1: Mix the glass, glaze or enamel binder and the absorbent uniformly, add the organic binder, and stir thoroughly to form a slurry, so that the absorbent in the slurry is evenly dispersed;
[0041] Step 2: Vacuum drying the slurry obtained in step 1 to obtain a green body with lower strength, use smelting crushing or sintering crushing process to prepare thermal spray powder; also use agglomeration sintering process to prepare powder, and spray the slurry Dry granulation treatment to obtain spherical powder, which can be used for thermal spraying after drying and light sintering.
[0042] Preferably, it can also include step 3: After the above step 2 is completed, the powder is processed by a flame spray gun or a plasma spray gun flame flow to make the glass cement material form a molten skeleton structure, and at ...
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[0052] Example 1: Preparation of low-melting glass and nickel-coated SiC absorbent system materials and coatings
[0053] Raw material: PbO 2 -SiO 2 Glass (average particle size <2μm) 400g, 30wt.% Ni-coated SiC powder (<14μm) 100g.
[0054] After the above-mentioned raw material powders are fully mixed, pure water and diluted polyvinyl alcohol solution (dilution ratio is about 10:1) are added, and the mixture is fully stirred, and the obtained slurry is fully dried in a vacuum drying box to form a dried body. , Put the green body into a vacuum sintering furnace, control the furnace temperature to 600℃, control the heating rate to 100℃ / 15min during the sintering process, and keep the temperature at 600℃ for 5h to ensure that the glass material is completely sintered. Crushing, pulverizing and sieving to obtain thermal spray powder materials with a particle size range of 45μm to 98μm. Use oxygen-acetylene flame spraying system to prepare the coating. Use flame spraying equipment wit...
Example Embodiment
[0055] Example 2:
[0056] Raw materials: 350g of phosphate glass powder (average particle size <3μm), 150g of FeNiCoAlSiRe alloy (~10μm).
[0057] Mix the above raw materials thoroughly, add a small amount of pure water to ensure that the solid content in the slurry is 50-65%, add 1-1.5% polyvinyl alcohol (PVA) as a binder during the stirring process, and use centrifugal spray drying granulation equipment Granulation process to obtain spherical powder, vacuum drying the powder at low temperature (100-150°C), sieving the dried powder, and finally obtaining spherical powder with a particle size between 25 μm and 53 μm. Using supersonic flame spraying equipment for spraying, a coating with a thickness of 1.2mm was prepared, and the peak reflectivity of the coating was (9.76GHz, -9.29dB). Coating bonding strength is 18MPa, when the coating thickness is 0.5mm, the areal density is 1.78Kg / m 2 . See the frequency-reflectance curve result of coating performance test Figure 4 , And its ...
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