Method and device for removing heavy metals in industrial wastewater by nanoscale zero-valent iron-multilevel reversed filter type system
A nano-zero-valent iron, industrial wastewater technology, applied in chemical instruments and methods, water/sewage multi-stage treatment, water pollutants, etc., can solve the problems of high cost and energy consumption, long operation time, complex equipment, etc. Simple structure, low cost and low energy consumption
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[0036] Example 1:
[0037] The nano zero-valent iron used in the present invention is FeCl 3 Solution and NaBH 4 It is prepared by mixing the solution and undergoing oxidation-reduction reaction. The particle size ranges from 1 to 100 nm, the average particle size is 30 to 70 nm, and the specific surface area is 20 to 40 m. 2 / g, such as figure 1 The structure model diagram of nano-zero-valent iron, a typical core-shell double structure, with dense zero-valent iron inside, which plays a reducing role; the outer ring is covered with a thin layer of iron oxide (or FeOOH) for adsorption. To synthesize the ready-to-use nano-zero-valent iron, add ethanol, isopropanol and other organic reagents to fluidize into the compact reaction zone of the closed reactor. The wet nano-zero-valent iron has a solid content of 20-80 g / L, and nano-zero Valence iron must be stored in an oxygen-free environment.
[0038] A method and device for removing medium and low-concentration heavy metal-containing...
Example Embodiment
[0043] Example 2:
[0044] Take a copper mine wastewater effluent stock solution, first pretreat the copper mine wastewater stock solution: add a certain amount of PAM flocculant, stir quickly for 1 to 2 minutes to make the added flocculant mix evenly in the solution, and then reduce the stirring speed to slow down Slowly agitate the mining wastewater for 30-60 minutes to condense the suspended impurities in the copper mine wastewater stock solution into flocs. After the flocculation is completed, stop the stirring, and let the electroplating wastewater settle for 1 to 3 hours. After the precipitation is completed, filter it with filter paper. Clarified electroplating wastewater. Mining wastewater after pretreatment contains Cu 2+ 200~800 mg / L, Ni 2+ 50~100 mg / L, Zn 2+ 10-30 mg / L, pH between 7-8.5. The nano zero-valent iron used in this example is made of 0.050 mol / LFeCl 3 Solution and 0.25 mol / LNaBH 4 Prepared by equal volume mixing reaction, the prepared nano-zero-valent iro...
Example Embodiment
[0047] Example 3:
[0048] Take the electroplating wastewater stock solution at the exit of the electroplating workshop of an electroplating factory, first pretreat the stock solution of electroplating wastewater: add a certain amount of PAM flocculant, first stir quickly for 1~2min to mix the added flocculant in the solution evenly, and then reduce the stirring speed. Slowly stir the electroplating wastewater for 30-60 minutes to condense the suspended impurities in the electroplating wastewater stock solution into flocs. After the flocculation is completed, stop the stirring, and let the electroplating wastewater settle for 1 to 3 hours. After the precipitation is completed, filter with filter paper to obtain a clarified Electroplating wastewater. The electroplating wastewater after pretreatment contains 300~800mg / L of Pb and Ni, and the pH is between 6~8. The nano zero-valent iron used in this example is made of 0.050mol / L FeCl 3 Solution and 0.25 mol / L NaBH 4 Prepared by e...
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