Production method of nitric oxide gas sensor element
A technology of gas sensors and nitrogen oxides, which is applied in the direction of instruments, scientific instruments, measuring devices, etc., to achieve the effect of less process conditions and easy control
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[0026] Example 1
[0027] 1) Wafer cleaning
[0028] Cut a 2-inch n-type single-sided polished single-crystal silicon wafer with a resistivity of 0.01Ω·cm, a thickness of 400±10μm and (100) crystal planes into a rectangular silicon substrate with a size of 2.2cm×0.8cm, and place them in sequence. Into acetone solvent, absolute ethanol and deionized water for ultrasonic cleaning for 20 minutes, then put it in a 5% hydrofluoric acid aqueous solution for 15 minutes, then rinse with deionized water, and finally put the silicon wafer Reserve in water and ethanol.
[0029] 2) Preparation of silicon-based porous silicon with ordered pores
[0030] The porous silicon layer was prepared on the polished surface of the silicon wafer by the double-slot electrochemical method. The corrosive liquid used is an aqueous solution of hydrofluoric acid with a mass fraction of 7%, and the applied corrosion current density is 125mA / cm 2 , The corrosion time is 20min. Prepared at room temperature and wit...
Example Embodiment
[0035] Example 2
[0036] This embodiment is similar to embodiment 1, except that: in step 2), the etching time of silicon-based porous silicon with ordered pores is 10 minutes, the average pore diameter is 82.07 nm, and the porosity is 48.78%. The obtained porous silicon The silicon gas sensor element is at room temperature to 1ppm NO 2 The gas sensitivity is 2.011.
Example Embodiment
[0037] Example 3
[0038] This embodiment is similar to embodiment 1, except that: in step 2), the etching time of silicon-based porous silicon with ordered pores is 15 minutes, and the measured average pore diameter is 112.25 nm, and the porosity is 68.75%. The silicon gas sensor element is at room temperature to 1ppm NO 2 The gas sensitivity is 2.395.
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