Preparation method of aggregation-induced emission molecule
A technique of aggregation-induced luminescence and molecules, applied in luminescent materials, chemical instruments and methods, and the preparation of amino compounds from amines, etc., can solve problems such as complex synthesis processes, achieve high fluorescence quantum yield, high yield, and good thermal stability sexual effect
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Embodiment 1
[0020] The synthesis of embodiment 1 compound 9-16
[0021] Synthetic roadmap as figure 1 shown.
[0022] (1) Under nitrogen or argon atmosphere, 1,4-dibromobenzene (4.72g, 20.0mmol) was dissolved in 60mL of anhydrous tetrahydrofuran (THF) and cooled at -78°C for half an hour. To the above solution, 9.2 mL of n-butyl lithium in n-hexane (n-BuLi, 2.3 M) was added dropwise. After low-temperature reaction for 1 hour, 50 mL of fluorenone (3.61 g, 20 mmol) in tetrahydrofuran (THF) was added, and the low-temperature reaction was continued for 3 hours, then it was allowed to rise to room temperature naturally, and stirred overnight. After the reaction, water was added to the reaction liquid, extracted with chloroform, and the organic phase was collected and dried over anhydrous sodium sulfate. Using petroleum ether and chloroform (v / v, 4 / 1) as the eluent, the product was chromatographed on a silica gel column, separated and purified, and dried in vacuo to obtain a pale yellow oil ...
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