Preparation method of colloidal solution of nano-ZnO
A nano-zinc oxide and colloidal solution technology, applied in the direction of zinc oxide/zinc hydroxide, nanotechnology, nanotechnology, etc., can solve the problems of easy agglomeration, difficult control of particle size by chemical methods, large size dispersion, etc., and achieve particle size Uniformity, good biocompatibility and biodegradability, viscosity reducing effect
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[0020] Example 1:
[0021] 1. Prepare dialdehyde-based hydroxypropyl cellulose according to the technical scheme provided in the literature "Selectively oxidize the aggregate structure of cotton fiber". The preparation method is: first dissolve hydroxypropyl methyl cellulose in deionized water to obtain the quality The percentage of 1% hydroxypropyl methylcellulose solution, and then the mass fraction of 1% sodium periodate aqueous solution is gradually dropped into the above solution, the volume ratio of the two is 1:1-50:1. The reaction temperature was set to 50°C, and the reaction was fully reacted with mechanical stirring under a dark environment. After 30 minutes of reaction, the reaction solution was cooled to room temperature. Then the above solution was dialyzed for 24 hours with a dialysis bag with a molecular weight of 5000 to obtain pure dialdehyde hydroxypropyl methylcellulose. See attached figure 1 , It is the infrared spectrum of hydroxypropyl methyl cellulose befo...
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[0028] Example 2:
[0029] 1. Prepare dialdehyde hydroxypropyl methylcellulose according to the technical scheme of Example 1. Dissolve 0.20 g of dialdehyde hydroxypropyl methylcellulose in 100 mL of deionized water to obtain an aqueous solution of dialdehyde hydroxypropyl methylcellulose with a concentration of 2 g / L;
[0030] 2. Dissolve 0.727g of zinc nitrate in 100mL of deionized water to obtain a zinc nitrate solution with a concentration of 7.27g / L;
[0031] 3. Dissolve 5g of sodium hydroxide in 100mL of deionized water to obtain an aqueous solution of sodium hydroxide with a concentration of 50g / L;
[0032] 4. Mix 2g / L dialdehyde hydroxypropyl methylcellulose aqueous solution and 7.87g / L zinc nitrate aqueous solution at a volume ratio of 4:1, and add 50g / L dropwise at 70°C under constant stirring. An aqueous solution of L sodium hydroxide (the mass ratio of zinc nitrate to sodium hydroxide is 189:80), after 2 hours of reaction, a nano-zinc oxide colloidal solution with a part...
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[0033] Example 3:
[0034] 1. Dissolve 0.20 g of dialdehyde hydroxypropyl methylcellulose in 100 mL of deionized water to obtain an aqueous solution of dialdehyde hydroxypropyl methylcellulose with a concentration of 2 g / L;
[0035] 2. Dissolve 0.727g of zinc nitrate in 100mL of deionized water to obtain a zinc nitrate solution with a concentration of 7.27g / L;
[0036] 3. Dissolve 5mL ammonia in 95mL deionized water to obtain an aqueous ammonia solution;
[0037] 4. Mix 2g / L dialdehyde hydroxypropyl methylcellulose aqueous solution and 7.87g / L zinc nitrate aqueous solution in a volume ratio of 4:1, and add ammonia aqueous solution dropwise at 70℃ under constant stirring. (The mass ratio of zinc nitrate to ammonia is 189:20). After 2 hours of reaction, a nano-zinc oxide colloidal solution with a particle size of 10-60 nm can be obtained.
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