Method for manufacturing field-effect transistor based on quantum dot film conducting channel
A conductive channel and field effect transistor technology, which is applied in semiconductor/solid-state device manufacturing, circuits, transistors, etc., can solve the problems of limited overall performance of the device, complicated manufacturing process, limited sensitivity, switching frequency and speed, etc., and achieve device performance Flexible and controllable, simple preparation process and novel preparation method
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Embodiment 1
[0033] (1) Weigh 10g of tri-n-octylphosphine oxide, 10g of octadecylamine and 0.5g of cadmium stearate, mix them and treat them under vacuum conditions at 100°C for 0.5 hours. Rise to 320°C to form a cadmium precursor solution;
[0034] (2) Weigh 0.625 mg of selenium powder and dissolve it in 5 ml of tributylphosphine under the protection of nitrogen atmosphere to form a selenium precursor solution;
[0035] (3) Rapidly inject the selenium precursor solution into the cadmium precursor solution, then lower the temperature of the mixed solution to 290 ° C, and keep it at this temperature for 10 hours; and use the chlorobenzene / methanol mixed solution to mix and centrifuge several times to Remove excess reactants and impurity ions to obtain CdSe quantum dot chlorobenzene solution, wherein the concentration of CdSe quantum dots is 5 / cm 3 ;
[0036] (4) Under a nitrogen atmosphere, mix 100 mM 16-mercaptohexadecanoic acid chlorobenzene solution with the prepared CdSe quantum dot chl...
Embodiment 2
[0042] (1) Weigh 20g of tri-n-octylphosphine oxide, 20g of octadecylamine and 2.1g of cadmium stearate, mix them and treat them under vacuum conditions at 115°C for 1.8 hours, then, under the protection of nitrogen atmosphere, the temperature Rise to 320°C to form a cadmium precursor solution;
[0043] (2) Weigh 9.75 mg of selenium powder and dissolve it in 10 ml of tributylphosphine under the protection of nitrogen atmosphere to form a selenium precursor solution;
[0044] (3) Rapidly inject the selenium precursor solution into the cadmium precursor solution, then lower the temperature of the mixed solution to 290 ° C, and keep it at this temperature for 15 hours; and use the chlorobenzene / methanol mixed solution to mix and centrifuge several times to Remove excess reactants and impurity ions, thereby obtaining CdSe quantum dot chlorobenzene solution, that is, the third mixed solution, wherein the concentration of CdSe quantum dots is 8 / cm 3 ;
[0045] (4) Under a nitrogen ...
Embodiment 3
[0051] (1) Weigh 30g of tri-n-octylphosphine oxide, 30g of octadecylamine and 3.7g of cadmium stearate, mix them and treat them under vacuum conditions at 130°C for 3 hours, then, under the protection of nitrogen atmosphere, the temperature Rise to 320°C to form a cadmium precursor solution;
[0052] (2) Under the protection of nitrogen atmosphere, 18.75 mg of selenium powder was weighed and dissolved in 15 ml of tributylphosphine to form a selenium precursor solution;
[0053] (3) Rapidly inject the selenium precursor solution into the cadmium precursor solution, then lower the temperature of the mixed solution to 290 ° C, and keep it at this temperature for 20 hours; and use the chlorobenzene / methanol mixed solution to mix and centrifuge for several times. Remove excess reactants and impurity ions to obtain CdSe quantum dot chlorobenzene solution, wherein the concentration of CdSe quantum dots is 10 / cm 3 ;
[0054] (4) Under a nitrogen atmosphere, mix 250 mM chlorobenzene ...
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