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Method for inspecting quality of slender acanthopanax stilbenes powder

A kind of Acanthopanax powder, quality technology, applied in the direction of measuring device, color/spectral characteristic measurement, instrument, etc., can solve the problems of unfavorable quality and no quality standard, and achieve the effect of safe clinical use and good accuracy

Inactive Publication Date: 2015-03-18
LUOYANG HUIZHONG ANIMAL MEDICINE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Wujiaqi powder is a traditional Chinese medicine immune enhancer developed according to traditional Chinese medicine theory. There is no quality standard, which is not conducive to its quality control. In order to ensure safe, effective and stable clinical use, it is necessary to establish a perfect quality standard and its testing methods

Method used

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  • Method for inspecting quality of slender acanthopanax stilbenes powder
  • Method for inspecting quality of slender acanthopanax stilbenes powder
  • Method for inspecting quality of slender acanthopanax stilbenes powder

Examples

Experimental program
Comparison scheme
Effect test

example 1

[0061] Example 1: Preparation of Acanthopanax powder

[0062] Acanthopanax powder: Prescription: Astragalus 800g, Acanthopanax 200g.

[0063] Preparation method: crush the above 2 traditional Chinese medicines into the coarsest powder, add 8 times the amount of water, soak for 1 hour, decoct and reflux for extraction for 2 hours, filter, add water to the filter residue and extract twice, add 8 times the amount of water each time and reflux for 2 hours , filtered several times, combined the filtrates, centrifuged while hot (50-60°C), concentrated the supernatant under reduced pressure to a relative density of about 1.2 (≤70°C), and spray-dried to obtain 300g of the finished product.

example 2

[0064] Example 2: Examination of the specificity of the identification method of Acanthopanax powder

[0065] (1) Reagents and samples

[0066] Control samples: Astragaloside IV, batch number: 110781-200613, purchased from China National Institutes for Food and Drug Control;

[0067] Acanthopanax powder: prepared in Example 1.

[0068] Negative control samples: Prepare negative control samples for each identification item according to the method in Example 1.

[0069] (2) Identification of Astragalus

[0070] Take 1 g of the sample prepared in Example 1, add 20 mL of methanol, heat and reflux for 1 hour, filter, add the filtrate to a neutral alumina column (100-120 mesh, 5 g, inner diameter 10-15 mm), wash with 100 mL of 40% methanol Remove, collect the eluent, evaporate to dryness, add 30 mL of water to the residue to dissolve, shake and extract with n-butanol saturated with water twice, 20 mL each time, combine the n-butanol solution, wash with water twice, 20 mL each tim...

example 3

[0073] Example 3: Methodological investigation on the content determination of astragaloside IV

[0074] (1) Instruments and reagents, samples

[0075] Instrument: high performance liquid chromatography, e2695 type, Waters Corporation, USA

[0076] Evaporative light scattering detector, type 2424, Waters Corporation, USA

[0077] Electronic Analytical Balance, Model AB135-S, Mettler Toledo

[0078] Reagents: Acetonitrile is chromatographically pure; water is double distilled water; other reagents are analytically pure.

[0079] Control sample: Astragaloside IV, batch number: 110781-200613, purchased from China National Institutes for Food and Drug Control.

[0080] Acanthopanax powder: prepared in Example 1.

[0081] (2) Chromatographic conditions

[0082] The chromatographic column is a Kromasil100-5C18 column (150×4.6mm, 5μm); the mobile phase is acetonitrile-water (35:65); detection by an evaporative light scattering detector, the temperature of the drift tube is 60°C,...

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Abstract

The invention relates to a method for inspecting the quality of slender acanthopanax stilbenes powder. The method comprises qualitative analysis and quantitative determination for the slender acanthopanax stilbenes powder. Compared with a method for inspecting the quality of a lingqijia oral solution, the method adopts a high performance liquid chromatography for measuring the content of astragaloside in the slender acanthopanax stilbenes powder, and a measuring method for the total sugar content is also adopted, a thin layer chromatography is adopted for respectively inspecting the astragaloside and isofraxidin in the slender acanthopanax stilbenes powder. The method is good in specificity, repeatability and accuracy and is used for performing comprehensive evaluation on the quality of the slender acanthopanax stilbenes powder so that the quality of a product is effectively controlled and safe, the effective and stable clinical use can be guaranteed.

Description

technical field [0001] The invention belongs to the technical field of detection of traditional Chinese medicines, and relates to a method for inspecting the quality of Acanthopanax powder. The method can be used for comprehensively evaluating the quality of Acanthopanax powder. Background technique [0002] With the development of intensification and industrialization of the breeding industry, the susceptibility of livestock and poultry to pathogenic microorganisms is increasing, and diseases occur frequently. In order to prevent and control diseases, the traditional method is to use a large amount of antibiotics. As a result, drug-resistant strains continue to increase, resulting in livestock Poultry immune function drops sharply, growth is hindered, and the abuse of antibiotics also leads to enhanced vaccination response, increased side effects or failure of immunization, causing great economic losses to the aquaculture industry. [0003] Immunopotentiators are a class of...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/31G01N21/33G01N30/90G01N30/02
Inventor 张许科刘兴金张晓会
Owner LUOYANG HUIZHONG ANIMAL MEDICINE
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