A kind of preparation method of ni3c magnetic nanowire
A magnetic nano, soluble technology, applied in the direction of nanotechnology, nanotechnology, nanotechnology for materials and surface science, etc., to achieve the effects of short synthesis cycle, easy large-scale production, and simple preparation process
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Embodiment 1
[0026] Embodiment 1: under room temperature condition, weigh 1.16 g Ni(NO 3 ) 2 ·6H 2 O, 0.1 g KOH, dissolved in a 90 mL tetraethylene glycol beaker, stirred vigorously under a magnetic stirrer, and the heating temperature was 40 °C, when the solute was completely dissolved, a green transparent solution was obtained, and at the same time, a certain amount of The ruthenium salt was added to a glass bottle of 5 ml alcohol solution, and the heating temperature was 100°C, so that it could be quickly dissolved for later use. The prepared green solution was transferred to a 250 mL four-neck flask, connected with a splash-proof ball and an air condenser, and heated to 100°C under the protection of an inert gas, and kept at 100°C for 40 minutes to remove the Moisture; under inert gas protection conditions, heat up at 2 °C / min, heat to 310 °C, reflux for 10 minutes, add surfactant 1ml, (V triphenylphosphine: V oleylamine = 0.5), continue to reflux for 3 hours . After the reaction, ...
Embodiment 2
[0027] Embodiment 2: Under room temperature condition, weigh 0.30g Ni(ac) 2 4H 2 O, 0.2g NaOH, dissolved in a 50 mL, 1,2-butanediol beaker, stirred vigorously under a magnetic stirrer, and the heating temperature was 40°C. When the solute was completely dissolved, a green transparent solution was obtained. At the same time, weigh Take a certain amount of ruthenium salt and add it to a 5 ml glass bottle of alcohol solution, and heat it at 100°C to dissolve it quickly for later use. The prepared green solution was transferred to a 100 mL four-neck flask, connected with a splash-proof ball and an air condenser, and under the protection of an inert gas, the temperature was raised to 100°C, and the temperature was kept at 100°C for 40 minutes to remove the Moisture; under inert gas protection conditions, heat up at 2°C / min, heat to 200°C, reflux for 20 minutes, add 0.5 ml of surfactant, (V triphenylphosphine: V oleylamine=1), continue to reflux for 3 hours . After the reaction, ...
Embodiment 3
[0028] Example 3: Weigh 0.30 g NiCl at room temperature 2 4H 2 O, 0.1g NaOH, dissolved in a 90 mL beaker of decanediol, stirred vigorously under a magnetic stirrer, the heating temperature was 40°C, when the solute was completely dissolved, a green transparent solution was obtained, and at the same time, weighed a certain amount of The ruthenium salt was added into a 10 ml glass bottle of alcohol solution, and the heating temperature was 100°C, so that it could be quickly dissolved for later use. The prepared green solution was transferred to a 250 mL four-neck flask, connected with a splash-proof ball and an air condenser, and heated to 100°C under the protection of an inert gas, and kept at 100°C for 40 minutes to remove the Moisture; under inert gas protection conditions, heat up at 5 °C / min, heat to 200 °C, reflux for 10 minutes, add surfactant 1ml, (V triphenylphosphine: V oleylamine = 1.5), continue to reflux for 20 min. After the reaction, cool to room temperature und...
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