A kind of environmental protection material containing diatom ooze and its preparation method and the use of preparation floor
An environmentally friendly material and diatom mud technology, which is applied in the fields of environmental protection materials and their preparation, and floor coating, can solve the problems that the functions need to be diversified and the performance needs to be improved, and achieve excellent protection and indoor purification. Widely industrialized application prospects and practical Value, excellent environmental protection effect
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preparation example 1
[0044] Preparation Example 1: Complex Auxiliary (Acetylacetonate Isoniazid Molybdenum Complex)
[0045] Add 1mol isonicotinic acid hydrazide and 30mol pyridine to the industrial reactor, heat up to 75°C, stir to dissolve, then add 1.5mol acetylacetone and stir for 1.5 hours, finally add 1mol molybdenum acetylacetonate and continue stirring for 2.5 hours, suction filtration, washing, Vacuum-dried to obtain the required complex auxiliary agent acetylacetonate isoniazid molybdenum complex, ready for use.
[0046] In all the following examples, unless otherwise specified, all "complex additives" are molybdenum complexes of isoniazid acetylacetonate prepared in this preparation example.
preparation example 2
[0047] Preparation Example 2: Fullerene Amine Adducts
[0048] Under a nitrogen atmosphere, add an appropriate amount of toluene to the reactor, then add 10mmol C60 fullerene and 150mmol N,N-dimethyl-1,3-diaminopropane, stir and dissolve, then heat to reflux for nitrogen-hydrogen addition reaction 12 hours, the reaction is over, cooled to room temperature, concentrated in vacuo, the residue is added to n-hexane for precipitation, and the precipitate is collected by filtration to obtain the desired fullerene adduct, which is set aside.
[0049] In all the following examples, unless otherwise specified, all "fullerene amine adducts" are the fullerene amine adducts prepared in this preparation example.
preparation example 3
[0050] Preparation Example 3: Plant Extract
[0051] In the industrial extraction kettle, adding completely dry chestnut flower and lavender with a mass ratio of 1:0.4 is a total of 500g, then adding 4500g of a mass ratio of N-butylpyridine tetrafluoroborate and ethanol mixed solvent at room temperature Extract under microwave power 280W for 25 minutes, then microwave, continue to heat to 65°C for extraction for 45 minutes, then filter and vacuum concentrate to 1 / 10 of the volume to obtain the plant extract for future use.
[0052] In all the following examples, unless otherwise specified, all "plant extracts" are plant extracts prepared in this preparation example.
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