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A sludge demulsifier and sludge recycling process

A demulsifier and oil sludge technology, which is used in sludge treatment, water/sludge/sewage treatment, dehydration/drying/concentrated sludge treatment, etc. problem, to achieve good demulsification effect, easy industrial application, and small environmental impact.

Active Publication Date: 2016-02-10
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The demulsifier has good interfacial activity and penetration ability, and has good demulsification ability for crude oil emulsion, but the preparation of the demulsifier is complicated, the cost is high, and it is not conducive to practical application
CN102041038A discloses a treatment method for heavy oil aging oil. The invention firstly provides a broken oil for heavy oil aging oil prepared by mixing phenol, styrene, polyethylene polyamine, formaldehyde, ethylene oxide and propylene oxide. Emulsion, the demulsifier has a good demulsification function and can achieve the destruction of the oil-water interface film, but the biodegradability is poor, and the subsequent impact on the environment is great

Method used

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  • A sludge demulsifier and sludge recycling process
  • A sludge demulsifier and sludge recycling process
  • A sludge demulsifier and sludge recycling process

Examples

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Effect test

Embodiment 1

[0034] Sodium fatty acid methyl ester sulfonate (R=C 16 ) 28 parts, alkyl polyglucoside (R=C 10 , n=3) 3 parts, 1 part of sodium citrate, and 68 parts of water were mixed in a reaction kettle at a temperature of 55°C for 40 minutes, and citric acid and sodium bicarbonate were added to adjust the pH value to 5-7 to obtain a sludge demulsifier.

Embodiment 2

[0036] Sodium fatty acid methyl ester sulfonate (R=C 16 ) 15 parts, alkyl polyglucoside (R=C 12 , n=3) 5 parts, 1 part of sodium citrate, and 79 parts of water were mixed in a reaction kettle at a temperature of 50°C for 35 minutes, and sorbic acid and sodium bicarbonate were added to adjust the pH value to 5-7 to obtain a sludge demulsifier.

Embodiment 3

[0038] Sodium fatty acid methyl ester sulfonate (R=C 14 ) 10 parts, alkyl polyglucoside (R=C 10 , n=2) 8 parts, 1 part of sodium citrate, and 81 parts of water were mixed in a reaction kettle at a temperature of 53°C for 35 minutes, and citric acid and sodium hydroxide were added to adjust the pH value to 5-7 to obtain a sludge demulsifier.

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Abstract

The invention discloses an oil sludge demulsifier and an oil sludge resourceful treatment process. The oil sludge demulsifier comprises the following components in parts by weight: 5-30 parts of fatty acid methyl ester sulfonate, 2-10 parts of alkyl polyglucoside, 0.5-2 parts of a green accessory ingredient and 58-92 parts of water. The oil sludge resourceful treatment process comprises the following steps: enabling oily sludge in a raw material storage sludge tank to enter a sludge mixing tank; adding the oil sludge demulsifier for demulsification treatment; enabling demulsified oily sludge to enter a stacked spiral type sludge dewatering machine for solid-liquid separation to obtain a filter liquor and a sludge cake; enabling the filter liquor to enter a gas-liquid mixing tank to be mixed with air; enabling the mixture to enter a separation tank for three-phase separation of oil, water and sludge. The oil sludge resourceful treatment process can reduce the moisture content of oily sludge from 80-98% to about 50%, can further recycle most crude oil in oily sludge, and greatly reduces the difficulty of sludge follow-up treatment. By combining the oil sludge demulsifier with the oil sludge demulsification process, the moisture content of oil sludge can be reduced from 80-98% to about 50%, most crude oil in oil sludge can be further recycled, and the difficulty of sludge follow-up treatment is greatly reduced.

Description

technical field [0001] The invention relates to an oil sludge demulsifier and a preparation method thereof, in particular to an environment-friendly oil sludge demulsifier containing fatty acid methyl ester sulfonate and a preparation method thereof; the invention also relates to an oil sludge recycling process. Background technique [0002] A large amount of black solid and semi-solid waste containing oil will be produced in the process of oil extraction, gathering and transportation, refining and oily sewage treatment, which is called oil sludge (referred to as oil sludge), and its main components are oil, mud and water. The size of solid particles in oil sludge can range from less than microns to several inches, most of which are between 1 and 100 microns. The composition of oil depends on the type of crude oil, refinery structure and operating conditions. The composition of sludge may change over time. According to statistics, China's annual output of oil sludge is nearl...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C02F11/14C02F1/40C02F1/52C10G1/00
CPCC02F1/40C02F1/5272C02F1/54C02F11/125C02F11/14C02F2303/06C10G1/00
Inventor 杨飞飞回军李宝忠赵景霞
Owner CHINA PETROLEUM & CHEM CORP
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