Method for preparing visual photonic crystal sensor
A technology of photonic crystals and sensing methods, which is applied in nanotechnology for sensing, measurement of color/spectral characteristics, analysis by making materials undergo chemical reactions, etc., can solve the problems of unfavorable rapid and effective detection, expensive equipment, and sensitivity Poor accuracy and other issues
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Embodiment approach 1
[0029] Embodiment 1: Preparation of phenylboronic acid group photonic crystal
[0030] Preparation of phenylboronic acid group photonic crystals: (1) After mixing a certain proportion of common functional monomers, suspension polymerization is carried out with 60mg initiator at 80°C and 370rpm for 45min to form monodisperse nanospheres.
[0031] (2) A certain proportion of common functional monomers are mixed (functional monomer methyl methacrylate is 3ml, isopropylacrylamide, 3-acrylamidophenylboronic acid common functional monomers are in a certain proportion), and the initiator is dissolved In 1.5ml of double-distilled water, the reaction was carried out in 27ml of double-distilled water.
[0032] (3) Screen the uniform particle size by gravity centrifugation, discard the supernatant and sediment, collect the emulsion, calculate its mass fraction, and prepare a certain concentration of monodisperse nano-microsphere emulsion.
[0033] (4) Preparation of photonic crystals by vertical...
Embodiment approach 2
[0040] Embodiment 2: Detection of glucose by photonic crystal sensor based on recognition of phenylboronic acid group with glucose
[0041] (1) Put the prepared photonic crystal under weak alkaline conditions (CHES Buffer with pH=8), and record the detection baseline after the fiber optic spectrometer is stable.
[0042] (2) Prepare 1, 5m mol / L glucose solution, and measure glucose from low concentration to high concentration (1-12, 15, 20m mol / L). After each sample addition, wait for 1-3min. After stabilization, record the detection response value ( Figure 5 , Image 6 ).
[0043] (3) Record the change of structural color before and after photonic crystal detection by digital camera (Cannon, Japan) ( Figure 7 ).
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