Oxidation-resistant high-heat-conductivity maleic-anhydride-grafted polyphenyl ether modified epoxy resin composite material for LED packaging and preparation method thereof
A technology of LED encapsulation and maleic anhydride, applied in the field of maleic anhydride grafted polyphenylene ether modified epoxy resin composite materials and its preparation, can solve the problem of UV resistance, poor aging resistance, high production cost, low cost, etc. problems, achieve good adhesion, long service life, and improve heat conduction
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[0011] The composite material of this embodiment is prepared from the following raw materials in parts by weight: bisphenol A type epoxy resin 70, polyphenylene ether powder 20, hydroxyl silicone oil 0.1, nano titanium dioxide 4, benzoyl peroxide 0.1, maleic anhydride 0.4 , Nano copper 0.1, colloidal graphite powder 0.2, silane coupling agent 0.1, chloroform amount, antioxidant 0.01, curing agent DDS20.
[0012] A method for preparing an oxidation-resistant and highly thermally conductive maleic anhydride grafted polyphenylene ether modified epoxy resin composite material for LED packaging, the preparation method is:
[0013] (1) Pre-irradiate the polyphenylene ether powder. The irradiation conditions are: use an electron accelerator as the irradiation source, and use β-rays to irradiate under normal temperature, normal pressure, and air atmosphere. The pre-irradiation dose range 20kGy, to obtain pre-irradiated polyphenylene ether material;
[0014] (2) Put the pre-irradiated...
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