Antibacterial coating and preparation method thereof
An antibacterial coating, acrylic emulsion technology, applied in antifouling/underwater coatings, coatings, latex paints, etc., can solve the problems of promotion resistance, high price, and blackening of sterilization delayed products
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[0041] 2. Preparation of antibacterial coating
[0042]
[0043] The preparation method of described antibacterial coating is characterized in that: comprises the steps:
[0044] (1) Control the stirring rate to 300-500rmp, add 24.5-34.8 parts of deionized water, 0.5-0.7 parts of thickener and 0.1-0.3 parts of PH regulator to the mixer in sequence, and stir for 5-10 minutes;
[0045] (2) Then increase the speed to 800-1000r / min, add 0.1-0.2 parts of wetting agent, 0.5-1 part of dispersant, 0.5-1 part of defoamer, 10-20 parts of titanium dioxide and 20-30 parts of carbonic acid Calcium, then increase the speed to 1800-2000r / min, stir for 15-20min;
[0046] (3) Finally, reduce the speed to 1000-1200r / min, add 20-30 parts of emulsion, 0.8-1.5 parts of film-forming aid and 1-2.5 parts of antifreeze in turn, stir for 10-15 minutes and sieve with 200-300 mesh , to obtain the product of the present invention.
[0047] (two) embodiment:
Embodiment 1
[0049] 1. Preparation of antibacterial emulsion
[0050]
[0051]
[0052]The described acrylic emulsion with antibacterial function is formulated according to the following steps:
[0053] 1) Preparation of quaternary ammonium antibacterial monomer:
[0054] In a three-neck flask equipped with a stirrer and a constant pressure funnel, add 100% propoxypyromellitic acid ester dimethacrylate at a speed of 200rmp, slowly add dimethylaminoethyl methacrylate dropwise at room temperature, 0.5 After the addition of h is completed, react at room temperature for 1.5 h, stop stirring, and obtain the quaternary ammonium salt antibacterial monomer.
[0055] 2) Preparation of acrylic emulsion with antibacterial function:
[0056] With stirrer, N 2 Add quaternary ammonium salt antibacterial monomer, methyl methacrylate, isobutyl methacrylate, butyl acrylate, acrylic acid, deionized water in the five-necked flask of conduit, constant pressure funnel and thermometer, stir 15min under...
Embodiment 2
[0064] 1. Preparation of antibacterial emulsion
[0065]
[0066] The described acrylic emulsion with antibacterial function is formulated according to the following steps:
[0067] 1) Preparation of quaternary ammonium antibacterial monomer:
[0068] In a three-necked flask equipped with a stirrer and a constant pressure funnel, add 1 portion of propoxypyromellitic acid dimethacrylate, the rotation speed is 300rmp, and slowly add dimethylaminoethyl methacrylate dropwise at room temperature, 0.8 After the addition of h is completed, react at room temperature for 1.8 h, stop stirring, and obtain a quaternary ammonium salt antibacterial monomer.
[0069] 2) Preparation of acrylic emulsion with antibacterial function:
[0070] With stirrer, N 2 Add quaternary ammonium salt antibacterial monomer, methyl methacrylate, isobutyl methacrylate, butyl acrylate, acrylic acid, deionized water in the five-necked flask of conduit, constant pressure funnel and thermometer, stir 25min u...
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