Remanufacturing method for scrap titanium chips through ball milling-equal channel angularpressing

An equal-channel corner and remanufacturing technology, which is applied in the direction of using liquid cleaning methods, cleaning methods and utensils, chemical instruments and methods, etc., can solve difficult microstructure refinement, strength loss, coarsening of ultrafine structure grains, etc. problems, achieve the effect of preventing continuous distribution and aggregation, simple and practical process operation, and excellent technical indicators

An equal-channel corner and remanufacturing technology, which is applied in the direction of using liquid cleaning methods, cleaning methods and utensils, chemical instruments and methods, etc., can solve difficult microstructure refinement, strength loss, coarsening of ultrafine structure grains, etc. problems, achieve the effect of preventing continuous distribution and aggregation, simple and practical process operation, and excellent technical indicators

CN105618501AInactive Publication Date: 2016-06-01SHANGHAI DIANJI UNIV

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  • Remanufacturing method for scrap titanium chips through ball milling-equal channel angularpressing

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Embodiment Construction

[0027] The preferred embodiments of the present invention are given below in conjunction with the accompanying drawings to describe the technical solution of the present invention in detail.

[0028] Step (1) - Ti chip recovery pretreatment:

[0029] Grade 2 Ti (ASTM Grade 2) chips generated by end milling were used as raw materials. After collecting the chips, the chemical composition (mass percentage, wt%) was analyzed by Inductively coupled plasma atomic emission spectroscopy (ICP-AES). The results are shown in Table 1. It can be seen from Table 1 that the chemical composition (such as oxygen content) of the Ti-2 chips processed by end milling meets the ASTM standard range. At the same time, 99.9% ethanol is used to clean Ti chips in an ultrasonic vibration tank to remove oil and impurities in raw materials.

[0030] Step (2) - BM treatment of Ti chips:

[0031] Put the Ti chips obtained from step (1) into a steel BM container, and the mass ratio between chips and steel ...

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Abstract

The invention provides a remanufacturing method for scrap titanium chips through ball milling-equal channel angular pressing. The remanufacturing method sequentially comprises the step of recovering and pretreating titanium chips, the step of performing ball milling treatment on the titanium chips, the step of loading the titanium chips into an equal channel angular pressing mold, the step of performing preprocessing at a room temperature through the equal channel angular pressing, the step of curing and processing at a high temperature, and the step of quenching. The ball milling-equal channel angular pressing composite technique provided by the invention is simple and practical to operate and high in controllability. Through remanufacturing, not only can nanometer block titanium materials (smaller than 200nanometers) with full densification be obtained, but also the metallurgical defect of the continuous distribution and gathering of large sliced oxides can be eliminated. In addition, the shapes of the titanium chips are refined and reformed, and anisotropy caused by deformation texture in hexagonal close packed titanium materials is restrained. The yield strength of the remanufactured nanometer titanium materials reaches to the level of 5-grade titanium, the distribution of nanometer particles of the oxides presents a dispersed uniform state, and through the isotropy of the properties of the materials, the remanufacturing of scrap titanium resources for value increase at low cost is realized.

Description

technical field [0001] The invention relates to the solid-state recycling and remanufacturing technology of waste titanium chips, in particular to a method for recycling waste titanium chips by adopting a ball milling-equal channel angular extrusion method. Background technique [0002] The recycling and remanufacturing of scrap metal resources is one of the key factors for achieving sustainable development. Titanium (Ti) is a very important metal resource with high smelting costs. It has excellent biocompatibility, good corrosion resistance, and suitable mechanical properties. It is an important material for the manufacture of medical devices, artificial joints, and large energy and chemical containers. However, in order to manufacture high-precision titanium structures, a large machining allowance needs to be designed. A considerable proportion of the raw material will be converted into waste swarf. The traditional chip treatment technology is high-temperature melting an...

Claims

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Application Information

Patent Timeline
01 Jun 2016
Publication
CN105618501A
IPC
B21C23/02; B21C23/32; B02C17/10; B08B3/12; B08B3/08; C22F1/18
CPC
B02C17/10; B08B3/08; B08B3/12; B21C23/001; B21C23/02; B21C23/32; C22F1/183
Inventors
罗蓬