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Wear-resistant and high temperature-resistant ceramic mold material and preparation method thereof

A technology for high-temperature resistant ceramics and mold materials, applied in the field of mold materials, can solve the problems of high product damage rate, easy cracking damage, short service life, etc., and achieve the effects of excellent thermal shock resistance, improved service life and good toughness.

Inactive Publication Date: 2016-07-20
吴申龙
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, traditional alloy molds generally have a short lifespan in high-temperature working environments, and are prone to cracking and damage under high temperature and long-term wear, resulting in a high damage rate of products and great losses

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] Wear-resistant and high-temperature resistant ceramic mold material, prepared from the following raw materials in parts by weight: 30 parts of magnesium aluminum silicate, 8 parts of nano-cerium dioxide, 6 parts of nano-zirconia, 30 parts of alumina, 26 parts of yttrium oxide, carbonized 28 parts of silicon, 3 parts of chromium, 6 parts of nickel, 40 parts of iron, 24 parts of copper, 12 parts of sulfur, 10 parts of borax, 20 parts of carbon fiber, 13 parts of tributyl tin trichloride, 17 parts of butyl methacrylate, 17 parts of ethylenediamine.

[0018] The preparation steps of above-mentioned mold material are as follows:

[0019] (1) After mixing the above raw materials according to the ratio, put them into a ball mill for ball milling for 8 hours to obtain a stable suspension slurry;

[0020] (2) Add tributyltin trichloride, butyl methacrylate and ethylenediamine to the slurry, and after ball milling for 30 minutes, vacuum defoaming for 12 minutes;

[0021] (3) In...

Embodiment 2

[0025] Wear-resistant and high-temperature resistant ceramic mold material, prepared from the following raw materials in parts by weight: 35 parts of magnesium aluminum silicate, 7 parts of nano-cerium dioxide, 7 parts of nano-zirconia, 25 parts of alumina, 27 parts of yttrium oxide, carbonized 26 parts of silicon, 4 parts of chromium, 5 parts of nickel, 45 parts of iron, 22 parts of copper, 13 parts of sulfur, 9 parts of borax, 22 parts of carbon fiber, 12 parts of tributyl tin trichloride, 18 parts of butyl methacrylate, 16 parts of ethylenediamine.

[0026] The preparation steps of above-mentioned mold material are as follows:

[0027] (1) After mixing the above raw materials according to the ratio, put them into a ball mill for ball milling for 9 hours to obtain a stable suspension slurry;

[0028] (2) Add tributyltin trichloride, butyl methacrylate and ethylenediamine to the slurry, and after ball milling for 35 minutes, vacuum defoaming for 11 minutes;

[0029] (3) Inj...

Embodiment 3

[0033] Wear-resistant and high-temperature resistant ceramic mold material, prepared from the following raw materials in parts by weight: 40 parts of magnesium aluminum silicate, 6 parts of nano-cerium dioxide, 8 parts of nano-zirconia, 20 parts of alumina, 28 parts of yttrium oxide, carbonized 24 parts of silicon, 5 parts of chromium, 4 parts of nickel, 50 parts of iron, 20 parts of copper, 14 parts of sulfur, 8 parts of borax, 24 parts of carbon fiber, 11 parts of tributyl tin trichloride, 19 parts of butyl methacrylate, 15 parts of ethylenediamine.

[0034] The preparation steps of above-mentioned mold material are as follows:

[0035] (1) After mixing the above raw materials according to the ratio, put them into a ball mill for ball milling for 10 hours to obtain a stable suspension slurry;

[0036] (2) Add tributyltin trichloride, butyl methacrylate and ethylenediamine to the slurry, and after ball milling for 30 minutes, vacuum defoaming for 12 minutes;

[0037] (3) In...

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Abstract

The invention discloses a wear-resistant and high temperature-resistant ceramic mold material and a preparation method thereof. The material is prepared by aluminum magnesium silicate, nanometer cerium dioxide, nanometer zirconium dioxide, aluminum oxide, yttrium oxide, silicon carbide, chromium, nickel, iron, copper, sulfur, borax, carbon fibers, tributyl tin trichloride, butyl methacrylate and ethylenediamine; the raw materials are put in a ball mill for ball milling to obtain stable suspension slurry after being mixed in proportion; tributyl tin trichloride, butyl methacrylate and ethylenediamine are added for ball milling and vacuum foam removal, are injected in a mold for in-situ solidification and colloidal molding, are dried at room temperature, are demolded and dried, are charged in a furnace, and remove glue in vacuum; nitrogen is introduced for heating and pressurization; the furnace is stopped through power failure; and the raw materials are discharged from the furnace after cooling to prepare the wear-resistant and high temperature-resistant ceramic mold material. The mold structure has excellent heat stability, wear resistance and high-temperature resistance, also has excellent toughness, thermal shock resistance and mechanical strength, and prominently prolongs the mold service life.

Description

technical field [0001] The invention relates to the field of mold materials, in particular to a wear-resistant and high-temperature resistant ceramic mold material and a preparation method thereof. Background technique [0002] Mold is playing an increasingly important role in my country's economic development and has been widely used in all walks of life. Mold molding has many advantages such as high efficiency, good quality, saving raw materials, and reducing costs. According to statistics, more than 60% of the parts of airplanes, tanks, automobiles, tractors, electrical appliances, instruments and meters, etc., and more than 85% of the parts of bicycles, washing machines, refrigerators, electric fans, air conditioners, cameras, etc. Mold production. Without molds, there would be no modern industrial development. All countries in the world attach great importance to the mold industry. [0003] Factors affecting the service life of the mold include design structure, form...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C29/00C22C30/02C22C1/05C22C1/10
CPCC22C29/00C22C1/05C22C30/02
Inventor 吴申龙
Owner 吴申龙
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