Surface treatment process of molybdenum foil for spaceflight interconnection piece
A technology of surface treatment and interconnection sheet, applied in metal material coating process, ion implantation plating, coating and other directions, can solve the problems of easy interface cracking, poor bonding force of molybdenum foil, mismatch of thermal expansion coefficient, etc., to avoid Secondary oxidation, low cost, enhanced binding effect
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Embodiment 1
[0017] The surface treatment process of molybdenum foil for aerospace interconnection sheet includes the following steps:
[0018] (1) Degreasing: Soak the molybdenum foil workpiece in acetone solution for 35 minutes, methanol solution for 10 minutes, isopropanol solution for 10 minutes, and blow dry with high pressure nitrogen;
[0019] (2) Pickling: Sulfuric acid and deionized water are prepared into an acid solution in a mass ratio of 1:5, and the degreasing treated molybdenum foil workpiece is immersed in the acid solution for 30 minutes to completely eliminate the surface oxide layer. Ionized water for 10min;
[0020] (3) Alkaline washing: Soak the pickled molybdenum foil workpiece in 50% NaOH solution at 75℃ for 60min, then transfer it to acetone solution for soaking within 5s, observe by atomic force microscope, the surface roughness is less than 100nm;
[0021] (4) Nickel-chromium alloy: at 10 -7 Under the vacuum degree of Torr, the molybdenum foil workpiece after a...
Embodiment 2
[0025] The surface treatment process of molybdenum foil for aerospace interconnection sheet includes the following steps:
[0026] (1) Degreasing: Soak the molybdenum foil workpiece in acetone solution for 40 minutes, methanol solution for 12 minutes, isopropanol solution for 12 minutes, and blow dry with high pressure nitrogen;
[0027] (2) Pickling: Sulfuric acid and deionized water are prepared into an acid solution in a mass ratio of 1:5, and the degreasing treated molybdenum foil workpiece is immersed in the acid solution for 30 minutes to completely eliminate the surface oxide layer. Ionized water cleaning for 12min;
[0028] (3) Alkaline washing: soak the pickled molybdenum foil workpiece in 50% NaOH solution at 80°C for 65min, then transfer it to acetone solution for soaking within 5s, observe by atomic force microscope, the surface roughness is less than 100nm;
[0029] (4) Nickel-chromium alloy: at 10 -7 Under the vacuum degree of Torr, the molybdenum foil workpiec...
Embodiment 3
[0033] The surface treatment process of molybdenum foil for aerospace interconnection sheet includes the following steps:
[0034] (1) Degreasing: soak the molybdenum foil workpiece in acetone solution for 45 minutes, methanol solution for 15 minutes, isopropanol solution for 15 minutes, and blow dry with high pressure nitrogen;
[0035] (2) Pickling: Sulfuric acid and deionized water are prepared into an acid solution in a mass ratio of 1:5, and the degreasing treated molybdenum foil workpiece is immersed in the acid solution for 35 minutes to completely eliminate the surface oxide layer. Ionized water for 15min;
[0036] (3) Alkaline washing: soak the pickled molybdenum foil workpiece in 50% NaOH solution at 85°C for 70min, then transfer it to acetone solution for soaking within 5s, observe by atomic force microscope, the surface roughness is less than 100nm;
[0037] (4) Nickel-chromium alloy: at 10 -6 Under the vacuum of Torr, the molybdenum foil workpiece after alkali ...
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