Quantum dot material, preparation method, quantum dot film, backlight module and display device
A quantum dot material and quantum dot technology, applied in the field of liquid crystal display, can solve the problems of easy agglomeration, uneven dispersion of quantum dots, high overlap rate of quantum dots, etc., and achieve the goal of reducing luminous efficiency, improving luminous efficiency, and reducing light loss Effect
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[0050] In the first aspect, an embodiment of the present invention provides a method for preparing a quantum dot material, see figure 2 , the preparation method comprises the following steps:
[0051] Step 1, mix silicate, organic solvent, silane coupling agent, polymer monomer, initiator and water evenly; polymer monomer is used to prepare transparent flexible polymer monomer, and initiator is used for catalytic Initiator for the polymerization of polymer monomers.
[0052] Step 2, adding quantum dots to the system obtained in step 1 and mixing uniformly; the quantum dots are quantum dots formed by II B group elements and VI A group elements and / or quantum dots formed by III A group elements and V A group elements .
[0053] In step 3, the system obtained in step 2 is reacted at a preset temperature for a preset time to form a wet gel.
[0054]In step 4, the wet gel obtained in step 3 is transformed into an aerogel by supercritical drying or freeze drying to obtain quantu...
Embodiment 1
[0086] An embodiment of the present invention provides a quantum dot material and a preparation method thereof. The quantum dot material uses silica / polymethyl methacrylate hybrid airgel as a matrix to load quantum dots, and utilizes the three-dimensional network structure of the airgel to make Quantum dots are evenly dispersed to prevent quantum dots from agglomerating. In the quantum dot material provided in this embodiment, the quantum dots used are CdSe / ZnS quantum dots with a core-shell structure, and the particle size of the quantum dots is 2-10 nm.
[0087] The preparation method of the quantum dot material provided in this embodiment is as follows:
[0088] Step 101, tetraethyl orthosilicate (TEOS), ethanol, γ-chloropropyl triethoxysilane (silane coupling agent KH550), methyl methacrylate (MMA), benzoyl peroxide and water according to The molar ratio is 1:0.2:0.05:0.5:0.25:2 for mixing.
[0089] In step 102, the materials in step 101 are uniformly mixed, and then the...
Embodiment 2
[0096] An embodiment of the present invention provides a quantum dot material and a preparation method thereof. The quantum dot material uses silica / polymethyl methacrylate hybrid airgel as a matrix to load quantum dots, and utilizes the three-dimensional network structure of the airgel to make Quantum dots are evenly dispersed to prevent quantum dots from agglomerating. In the quantum dot material provided in this embodiment, the quantum dots used are CdTe quantum dots, and the particle size of the quantum dots is 2-10 nm.
[0097] The preparation method of the quantum dot material provided in this embodiment is as follows:
[0098] Step 201, mix tetraethyl orthosilicate (TEOS), methanol, γ-chloropropyltrimethoxysilane, methyl methacrylate (MMA), azobisisobutyronitrile and water in a molar ratio of 1:0.1:0.02 :0.3:0.15:1 ratio for mixing.
[0099] In step 202, the materials in step 201 are mixed uniformly, and then the above-mentioned CdTe quantum dots are added thereto.
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