Preparation method of ultra-dispersed MoS2/rGO nano hybridization water-electrolysis hydrogen production catalyst
A technology of ultra-dispersion and electrolysis of water, applied in the direction of physical/chemical process catalysts, chemical instruments and methods, electrolysis process, etc., can solve the difficult problems of molybdenum disulfide/tungsten loading, achieve simple and fast synthesis process, and solve poor conductivity Effect
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[0033] Further, a hyperdisperse MoS 2 The preparation method of rGO nano-hybrid electrolysis water hydrogen production catalyst comprises the following steps:
[0034] 1) Synthesis of graphene oxide: Graphene oxide was synthesized from graphite powder by the Hummers method;
[0035] 2) UDSL-MoS 2 / Synthesis of rGO: prepared by hydrothermal synthesis with molybdate, cysteine and graphene oxide.
Embodiment
[0038] Synthesis of graphene oxide: by modified Hummers method (Marcano D C et al. , 2010) synthesized graphene oxide with natural graphite powder, the detailed process is as follows: first, 2.00 g of natural flake graphite powder was ground with 40 g of NaCl for 15 minutes, washed thoroughly with distilled water, and dried in a blast oven at 70 °C for 30 minutes. Place the treated graphite powder in 46 mL of concentrated H 2 SO 4 (98%), mechanically stirred for 24 hours. In a water bath at 40°C, add 1 g NaNO 3 , continue to stir for 5min; under ice-water bath, slowly add 6g KMnO 4 , stirring constantly, during this process the temperature of the mixture was kept not to exceed 20°C. Then, under a water bath at 40°C, stirring was continued for 30 min. Then 80 mL of distilled water was slowly added to the above mixture, at this time, the temperature of the reaction solution rose rapidly to 98° C., and stirred for 15 min. After the reaction is over, add 280mL distilled wat...
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