A kind of low thermal conductivity insulation material, its preparation method and its application
A thermal insulation material and low thermal conductivity technology, applied in the field of thermal insulation materials, can solve problems such as low density, achieve low cost, excellent grinding effect, increase softening degree and internal porosity
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Embodiment 1
[0036] A low thermal conductivity thermal insulation material, and its preparation method includes the following steps:
[0037] (1) Add 100 parts of corn stover powder, 230 parts of ethanol, 90 parts of water, and 50 parts of ethyl acetate to the reaction kettle, and react for 20 minutes at a reaction temperature of 27°C and a stirring speed of 95r / min to obtain a mixture ;
[0038] (2) Transfer the mixture to the freezer, and freeze the mixture at -45°C for 3 hours to obtain the frozen mixture;
[0039] (3) After pulverizing the frozen mixture, put it into a ball mill, the cylinder speed is 50r / min and react for 15 minutes, and pass through an 8000 mesh screen to obtain the frozen mixture powder;
[0040] (4), 470 parts of frozen mixture powder, 12 parts of orthosilicic acid, 4 parts of ammonium polyphosphate (manufacturer: Yunnan Tianyao Chemical Co., Ltd., model: TY-1324), 3 parts of sodium benzoate, 21 parts of chlorinated Ammonium and 10 parts of ammonium oxalate are added to t...
Embodiment 2
[0045] A low thermal conductivity thermal insulation material, and its preparation method includes the following steps:
[0046] (1) Add 100 parts of wheat straw powder, 180 parts of isopropanol, 70 parts of water, and 30 parts of butyl acetate to the reactor, and react for 10 minutes at a reaction temperature of 3°C and a stirring speed of 85r / min to obtain Mixture;
[0047] (2) Transfer the mixture to the freezer, and freeze the mixture at -15℃ for 5 hours to obtain the frozen mixture;
[0048] (3) After crushing the frozen mixture, put it into a ball mill, the cylinder speed is 37r / min and react for 20 minutes, and pass through an 8000 mesh screen to obtain the frozen mixture powder;
[0049] (4) Add 380 parts of frozen mixture powder, 8 parts of orthosilicic acid, 2 parts of magnesium hydroxide, 1 part of sodium benzoate, 10 parts of hydrochloric acid, and 3 parts of potassium oxalate to the reactor, and control the temperature to 60°C, Under the condition of stirring speed of 10...
Embodiment 3
[0054] A low thermal conductivity thermal insulation material, and its preparation method includes the following steps:
[0055] (1) Add 100 parts of tree powder, 300 parts of ethanol, 150 parts of water, and 90 parts of ethyl acetate to the reaction kettle, and react for 10 minutes at a reaction temperature of 45°C and a stirring speed of 120r / min to obtain a mixture;
[0056] (2) Transfer the mixture to the freezer, and freeze the mixture at -80℃ for 0.5h to obtain the frozen mixture;
[0057] (3) After crushing the frozen mixture, put it into a ball mill, the cylinder speed is 60r / min and react for 5 minutes, and pass through an 8000 mesh screen to obtain the frozen mixture powder;
[0058] (4), 640 parts of frozen mixture powder, 23 parts of orthosilicic acid, 5 parts of magnesium hydroxide, 3 parts of sodium pentachlorophenate (manufacturer: Guangzhou Sanchang Chemical Co., Ltd.), 30 parts of ammonium chloride, 13 parts Add a portion of ammonium oxalate to the reaction kettle, co...
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