Liquid metal thermal interface material with anti-fusing characteristic and preparation method of liquid metal thermal interface material
A thermal interface material, liquid metal technology, applied in the direction of semiconductor/solid-state device parts, circuits, electric solid-state devices, etc., can solve the problems of electronic chip short circuit, lateral leakage, etc., to eliminate short circuit, low production cost, excellent thermal conductivity Effects on performance and chemical stability
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Embodiment 1
[0032] Example 1: Preparation of the liquid metal thermal interface material 1 of the present invention.
[0033] Alloy raw materials were prepared in the following weight percentages: 22wt% indium, 1.4wt% bismuth, 0.3wt% antimony, 1.6wt% zinc, 0.05wt% silver, 0.02wt% nickel, 0.02wt% cerium, 0.01wt% europium, Sn was margin.
[0034] The above-mentioned proportioned alloy is melted by induction in a graphite crucible, and argon or nitrogen is used as a protective atmosphere. The temperature was kept at 420° C., and electromagnetic stirring was used for 10 minutes for sufficient homogenization. Then pour the melted alloy liquid into the graphite mold for casting. After the alloy is solidified, the alloy ingot is heat treated at 40°C for 3 hours to ensure that the second phase in the alloy is completely precipitated and the alloy has excellent mechanical properties. Then carry out cold rolling at room temperature, and roll to a thickness of 0.05 mm after several rollings, and ...
Embodiment 2
[0036] Example 2: Preparation of the liquid metal thermal interface material 2 of the present invention.
[0037] Alloy raw materials were prepared in the following weight percentages: 28wt% indium, 1.9wt% bismuth, 0.4wt% antimony, 1.8wt% zinc, 0.03wt% silver, 0.01wt% nickel, 0.01wt% cerium, 0.02wt% europium, Sn was margin.
[0038] The above-mentioned proportioned alloy is melted by induction in a graphite crucible, and argon or nitrogen is used as a protective atmosphere. The temperature was kept at 420° C., and electromagnetic stirring was used for 10 minutes for sufficient homogenization. Then pour the melted alloy liquid into the graphite mold for casting. After the alloy is solidified, the alloy ingot is heat treated at 80°C for 3 hours to ensure that the second phase in the alloy is completely precipitated and the alloy has excellent mechanical properties. Then carry out cold rolling at room temperature, and roll to a thickness of 0.05 mm after several rollings, and ...
Embodiment 3
[0040] Embodiment 3: Preparation of the liquid metal thermal interface material 3 of the present invention.
[0041] Alloy raw materials were prepared in the following weight percentages: 32wt% indium, 2.1wt% bismuth, 0.6wt% antimony, 2.9wt% zinc, 0.02wt% silver, 0.03wt% nickel, 0.02wt% cerium, 0.01wt% europium, Sn was margin.
[0042] The above-mentioned proportioned alloy is melted by induction in a graphite crucible, and argon or nitrogen is used as a protective atmosphere. The temperature was kept at 420° C., and electromagnetic stirring was used for 10 minutes for sufficient homogenization. Then pour the melted alloy liquid into the graphite mold for casting. After the alloy is solidified, the alloy ingot is heat treated at 100°C for 3 hours to ensure that the second phase in the alloy is completely precipitated and the alloy has excellent mechanical properties. Then carry out cold rolling at room temperature, and roll to a thickness of 0.05 mm after several rollings, ...
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