Method for synthesizing titanium dioxide/ titanium disulfide composite material by using one-step vulcanization method
A technology of titanium dioxide and composite materials, applied in the direction of titanium dioxide, titanium oxide/hydroxide, titanium sulfide, etc., can solve the problems of high experimental conditions, impure products, low yield, etc., and achieve high material purity and uniform shape , The effect of simple preparation method
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0043] 1) Weigh 2ml of butyl titanate and add it dropwise to 8ml of ethanol solution under the action of magnetic stirring to form a homogeneous mixture A, then add 1ml of ethanol to 40ml of deionized water under the action of magnetic stirring to form a uniform mixed solution b.
[0044] 2) The mixed solution A is added dropwise into the mixed solution B under the action of stirring, and then ultrasonicated for 0.5 h to obtain a transparent solution C. In addition, 0.1 mol / L HCl was added to adjust the pH value to 6 to obtain solution D.
[0045] 3) The solution D is added into the polytetrafluoroethylene lining, the filling ratio is controlled at 40%, the reaction temperature is controlled at 160°C, and the reaction time is controlled at 12h.
[0046] 4) After the reaction is completed, centrifuge and wash 3 times with deionized water and ethanol respectively. After vacuum drying at 80°C for 6 h, TiO was obtained by grinding 2 Precursor.
[0047] 5) Weigh a certain amoun...
Embodiment 2
[0052] 1) Weigh 4ml of butyl titanate and add it dropwise to 9ml of ethanol solution under the action of magnetic stirring to form a homogeneous mixture A, then add 2ml of ethanol to 40ml of deionized water under the action of magnetic stirring to form a uniform mixed solution b.
[0053] 2) The mixed solution A is added dropwise into the mixed solution B under the action of stirring, and then ultrasonicated for 1.5 hours to obtain a transparent solution C. In addition, 0.1 mol / L HCl was added to adjust the pH value to 6 to obtain solution D.
[0054] 3) The solution D is added to the polytetrafluoroethylene lining, the filling ratio is controlled at 50%, the reaction temperature is controlled at 180°C, and the reaction time is controlled at 16h.
[0055] 4) After the reaction is completed, centrifuge and wash 5 times with deionized water and ethanol respectively. After vacuum drying at 80 °C for 8 h, TiO was obtained by grinding 2 Precursor.
[0056] 5) Weigh a certain am...
Embodiment 3
[0062] 1) Weigh 6ml of butyl titanate and add it dropwise to 10ml of ethanol solution under the action of magnetic stirring to form a homogeneous mixture A, then add 3ml of ethanol to 40ml of deionized water under the action of magnetic stirring to form a uniform mixed solution b.
[0063] 2) The mixed solution A is added dropwise into the mixed solution B under the action of stirring, and then the transparent solution C is obtained by ultrasonication for 2 hours. In addition, 0.1 mol / L HCl was added to adjust the pH value to 6 to obtain solution D.
[0064] 3) The solution D is added into the polytetrafluoroethylene lining, the filling ratio is controlled at 60%, the reaction temperature is controlled at 200° C., and the reaction time is controlled at 20 h.
[0065] 4) After the reaction is completed, centrifuge and wash 6 times with deionized water and ethanol respectively. After vacuum drying at 80°C for 10 h, TiO was obtained by grinding 2 Precursor.
[0066] 5) Weigh ...
PUM
Login to view more Abstract
Description
Claims
Application Information
Login to view more - R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap