Method, vectors and kit for detection of protein interactome
A detection method and protein technology, applied in the field of systems biology research, can solve problems such as the inability to detect correlations and the inability to detect the interaction network of multiple proteins, and achieve the effect of improving throughput
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Embodiment 1
[0142] 1. Experimental materials and preparation
[0143] 1. Protein Interaction Footprinting (PiF)
[0144] (1) Strains and vectors
[0145] Cloned strain: Escherichia coli K12 strain DH5α (Sangon Biotech, SD8411)
[0146] Expression strain: Escherichia coli K12 strain JM109 (Takara, D9052A)
[0147] Carrier:
[0148] Based on pSP73 (Promega, P2221) and
[0149] pSB1K3 (iGEM Distribution)
[0150] culture medium
[0151] LB liquid medium:
[0152] Sodium chloride 1g, yeast extract 0.5g, peptone 1g, double distilled water 100ml
[0153] LB solid medium:
[0154] Sodium chloride 1g, yeast extract 0.5g, peptone 1g, agar 1.2g, double distilled water 100ml
[0155] M9 histidine-deficient medium:
[0156] Solution A: 2ml of 20% glucose solution, 1ml of 20mM adenine solution, 10ml of 10X histidine deficient amino acid supplement solution B: 0.1ml of 1M magnesium sulfate solution, 0.1ml of 1M thiamine hydrochloride solution, 0.1ml of 10mM zinc sulfate solution, 0.1ml of 10...
Embodiment 2
[0262] Example 2 Using PiF technology to simultaneously detect the homodimeric interaction of two different proteins in a cell
[0263] 1. Design of detection DNA sequence
[0264] In order to detect the homodimerization of two different proteins at the same time, two different proteins were constructed as fusion proteins with DNA-binding domains CI(N,wt) and CI(N,mut), so there are two DNA-binding structures in this detection system The domain dimerization combinations are CI(N,wt)CI(N,wt) and CI(N,mut)CI(N,mut). Based on this, two DNA sequences were designed and screened to specifically bind to the dimerization combinations of the above DNA-binding domains.
[0265] (1) Calculate the protein-DNA complex interaction energy
[0266] According to the steps described in the technical implementation, we downloaded the three-dimensional structure data of the CI(N,wt) dimer-DNA complex from the PDB database (PDB number: 1LMB), and used FoldX to calculate a series of DNA sequences...
Embodiment 3
[0333] Example 3 Using PiF technology to simultaneously detect three different protein interactions in a cell
[0334] 1. Design of detection DNA sequence
[0335] On the basis of Example 2, in addition to the homodimeric interactions of two proteins, we also need to simultaneously detect the heterodimeric interactions of two proteins, that is, to simultaneously detect three interactions between two proteins. Therefore, we need to design specific binding DNA sequences for the DNA-binding domain dimerization combination CI(N,wt)CI(N,mut).
[0336] (1) Calculation of protein-DNA interaction energy
[0337] Similar to Example 2, we used FoldX to calculate the interaction of a series of protein-DNA complexes containing DNA sequence point mutations compared with wild-type based on the structural data of the DNA-binding domain heterodimer-DNA complex can change (such as Figure 14 shown).
[0338] (2) Design of core sequence
[0339] Based on the calculation results of the abov...
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