Preparation method of modified-porous-carbon-fiber-loaded calcium chloride hygroscopic material

A technology of porous carbon fiber and hygroscopic material, which is applied in the direction of carbon fiber, fiber chemical characteristics, fiber treatment, etc. It can solve the problems of low adsorption performance, difficulty in recycling, poor interfacial bonding between materials, etc., and achieve high hygroscopic strength and low cost of use , the effect of fast carbonization speed

Active Publication Date: 2018-04-20
MAANSHAN XINZHOU GRAPES PROFESSIONAL COOP
View PDF7 Cites 3 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, the commonly used hygroscopic materials are divided into disposable hygroscopic materials and hygroscopic materials that can be used repeatedly. Among them, the most widely used hygroscopic materials are quicklime. Effect, its advantages are low price and large moisture absorption capacity, but the disadvantage is that it is disposable, and after moisture absorption, it becomes a strong alkaline powder, which is difficult to recycle. If it is not disposed of in time, the absorbed moisture will still be released.
[0005] At the same time, because the carbon fiber preparation process includes carbonization or graphitization, the carbon atom stacking orientation on the carbon fiber surface is more consistent, and the atomic layer spacing is smaller, so the fiber surface is non-polar and chemically inert. In addition, the carbon fiber surface has hydrophobic, Shortcomings such as smoothness and low adsorption performance lead to poor interfacial bonding between carbon fiber and its composite material

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0021] A method for preparing a modified porous carbon fiber loaded calcium chloride hygroscopic material, comprising the following steps:

[0022] (1) Mix calcium chloride and sodium carboxymethylcellulose at a mass ratio of 5:1 and dissolve in water with 2.5 times the mass to obtain a mixed salt solution for later use;

[0023] (2) Put the spinning solution in the electrospinning apparatus, wrap the receiver with aluminum foil, and collect the as-spun fibers on the aluminum foil. The process parameters of the spinning process are positive pressure 15kV, negative pressure 1.5kV, and advance rate 0.04 mm / min, the receiving rate is 30r / min, the distance between the needle and the receiver is 15cm, and the ambient temperature is 30°C. After the spinning is completed, let it stand at room temperature for one day to obtain the as-spun fiber, and then place it in an oven to raise the temperature. Solidify at 160°C for 60 minutes, take it out and put it into a tube furnace, raise th...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention discloses a preparation method of a modified-porous-carbon-fiber-loaded calcium chloride hygroscopic material. The hygroscopic material is made from calcium chloride, sodium carboxymethylcellulose, diatomite powder, coconut shell, phenol, and polyvinyl alcohol. Porous carbon fiber made from coconut shell undergoes multiple modification treatment. The obtained porous carbon fiber is high in mechanical strength and good in adsorbability. The porous carbon fiber itself can adsorb a large amount of water vapour from air, and the porous structure is beneficial for loading calcium chloride. The composite material is good in moisture absorption, and a small amount of added nanometer diatomite provides components with better adhesion and support after moisture absorption, which is beneficial for reuse of the hygroscopic material after high-temperature drying. The hygroscopic material is non-pollution to the environment, is low in application cost, and is super high in economic value and environmental value.

Description

technical field [0001] The invention relates to the technical field of thermal insulation materials, in particular to a preparation method of a modified porous carbon fiber-loaded calcium chloride hygroscopic material. Background technique [0002] Hygroscopic materials refer to substances that can absorb moisture from the air. Commonly used solid hygroscopic materials include silica gel, alumina, molecular sieves, etc. These substances have a strong affinity for moisture. Hygroscopic materials are used in a wide range of applications. They can be placed in the closet to absorb moisture and prevent clothes from becoming moldy and smelly. They can be placed in the car to absorb moisture and odors in the car. They can also be placed in the room to absorb moisture in the air and reduce Indoor humidity. [0003] At present, the commonly used hygroscopic materials are divided into disposable hygroscopic materials and hygroscopic materials that can be used repeatedly. Among them,...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): D06M11/155D06M15/09D06M11/71D06M11/79D01F9/24D01D1/02D01D5/00D06M101/40
CPCD01D1/02D01D5/003D01D5/0092D01F9/24D06M11/155D06M11/71D06M11/79D06M15/09D06M2101/40
Inventor 孙仁贵
Owner MAANSHAN XINZHOU GRAPES PROFESSIONAL COOP
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products