Deoxidant for oil-displacing polymer and preparation method of deoxidant
An oil-displacing polymer and oxygen scavenger technology, applied in the field of oilfield chemistry, can solve problems such as the decrease of residual oxygen concentration, the destruction of polymer molecular structure, and the decrease of polymer viscosity.
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[0008] (1) Preparation of carbohydrazide sulfate
[0009] The sulfuric acid solution was added dropwise to the carbohydrazide solution, stirring while dripping, after the addition, the precipitate was filtered and dried to obtain carbohydrazide sulfate; the concentration of sulfuric acid was 100~500g / L, and the concentration of carbohydrazide was 50~ 400g / L, the molar ratio of carbohydrazide to sulfuric acid is 1:(0.5~3);
[0010] (2) Preparation of oxygen scavenger microcapsules
[0011] Dissolve hydroxypropyl methyl cellulose phthalate in acetone, add carbohydrazide sulfate, thiourea and erythorbic acid to the acetone solution of hydroxypropyl methyl cellulose phthalate, Ultrasonic dispersion, the obtained system is the dispersed phase; the concentration of hydroxypropyl methyl cellulose phthalate in acetone is 50 ~ 250 g / L, carbamoyl sulfate and hydroxypropyl methyl cellulose phthalate The mass ratio of acid ester is 1:(0.04~1), and the mass ratio of carbhydrazide sulfate, thiou...
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[0028] The experimental methods used in the following examples are conventional methods unless otherwise specified.
[0029] The materials and reagents used in the following examples can be obtained from commercial sources unless otherwise specified.
[0030] The present invention will be further described below in conjunction with specific embodiments, but the protection scope of the present invention is not limited to this.
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[0031] Example 1:
[0032] An oxygen scavenger for oil-displacing polymers and a preparation method thereof, including the following steps:
[0033] (1) Preparation of carbohydrazide sulfate
[0034] Dissolve 20g carbohydrazide in 100mL water to prepare a carbohydrazide solution; dissolve 45g sulfuric acid in 180mL water to prepare a sulfuric acid solution; add the sulfuric acid solution dropwise to the carbohydrazide solution, and stir while dripping. After the addition is complete, the precipitation Filter and dry to obtain carbohydrazide sulfate;
[0035] (2) Preparation of oxygen scavenger microcapsules
[0036] Dissolve 10g of hydroxypropyl methylcellulose phthalate in 60mL of acetone, add 25g of carbhydrazide sulfate, 7.5g of thiourea and 3.5g of isoascorbic acid to the hydroxypropyl methylcellulose phthalate Disperse the acid ester in acetone solution ultrasonically to obtain the dispersed phase;
[0037] Dissolve 10g Span-80 and 1.2g magnesium oleate in 450mL No. 5 white oil to...
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