A kind of method and application of using water hyacinth to prepare porous carbon material
A technology of porous carbon materials and water hyacinth, applied in chemical instruments and methods, carbon compounds, water/sewage treatment, etc., can solve the problems of anaerobic environment of water body, low added value of utilization, and disappearance of biological communities, etc., and achieve specific surface area The effect of large and rich pore structure
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Embodiment 1
[0029] A kind of method utilizing water hyacinth to prepare porous carbon material, comprises the following steps:
[0030] (1) Pretreatment of water hyacinth: take the stem of water hyacinth, wash it, and air-dry it naturally for 5-6 days, then dry it in an oven at 105°C for 24 hours, then crush the dried stem of water hyacinth with a pulverizer, and dry it for 40 Mesh sieve;
[0031] (2) Hydrothermal treatment: Weigh 6.0 g of water hyacinth powder in step (1), add 60 mL of deionized water into a hydrothermal reaction kettle, and mix well; then place the reaction kettle at a temperature of 200° C. After the reaction, filter and dry to obtain lignite-like biomass hydrothermal carbon;
[0032] (3) Molten salt activation treatment: take 2.0g of hydrothermal carbon obtained in step (2), add 8.0gNa 2 CO 3 -K 2 CO 3 Mix the salt, put it in a corundum porcelain boat after mixing evenly, put it in a tube furnace, and put it in the N 2 Under the protection of gas, calcined at 85...
Embodiment 2
[0035] A kind of method utilizing water hyacinth to prepare porous carbon material, comprises the following steps:
[0036] (1) Pretreatment of water hyacinth: take the stem of water hyacinth, wash it, and air-dry it naturally for 5-6 days, then dry it in an oven at 105°C for 24 hours, then crush the dried stem of water hyacinth with a pulverizer, and dry it for 40 Mesh sieve;
[0037] (2) Hydrothermal treatment: Weigh 6.0g of water hyacinth powder in step (1), add 30mL of deionized water into the hydrothermal reaction kettle, mix well; then place the reaction kettle at 200°C for hydrothermal reaction for 24h , filter and dry after the reaction to obtain lignite-like biomass hydrothermal carbon;
[0038] (3) Molten salt activation treatment: take 2.0g of hydrothermal carbon obtained in step (2), add 8.0gNa 2 CO 3 -K 2 CO 3 Mix the salt, put it in a corundum porcelain boat after mixing evenly, put it in a tube furnace, and put it in the N 2 Under the protection of gas, ca...
Embodiment 3
[0041] A kind of method utilizing water hyacinth to prepare porous carbon material, comprises the following steps:
[0042] (1) Pretreatment of water hyacinth: take the stem of water hyacinth, wash it, and air-dry it naturally for 5-6 days, then dry it in an oven at 105°C for 24 hours, then crush the dried stem of water hyacinth with a pulverizer, and dry it for 40 Mesh sieve;
[0043] (2) Hydrothermal treatment: Weigh 6.0g of water hyacinth powder in step (1), add 60mL of deionized water into the hydrothermal reaction kettle, mix well; then place the reaction kettle at 180°C for hydrothermal reaction for 24h , filter and dry after the reaction to obtain lignite-like biomass hydrothermal carbon;
[0044] (3) Molten salt activation treatment: take 2.0g of hydrothermal carbon obtained in step (2), add 8.0gNa 2 CO 3 -K 2 CO 3 Mix the salt, put it in a corundum porcelain boat after mixing evenly, put it in a tube furnace, and put it in the N 2 Under the protection of gas, ca...
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