Chemical nickel-plating-molybdenum-phosphorus alloy solution for preparing high molybdenum and high phosphorus coating
What is Al technical title?
Al technical title is built by PatSnap Al team. It summarizes the technical point description of the patent document.
A technology of electroless nickel plating and alloy solution, applied in liquid electroless plating, coating, metal material coating process, etc., can solve the problem of not being able to prepare Mo and P content at the same time, achieve good diffusion barrier performance and improve reliability , the effect of high thermal stability
Inactive Publication Date: 2018-07-13
SHENYANG POLYTECHNIC UNIV
View PDF7 Cites 3 Cited by
Summary
Abstract
Description
Claims
Application Information
AI Technical Summary
This helps you quickly interpret patents by identifying the three key elements:
Problems solved by technology
Method used
Benefits of technology
Problems solved by technology
[0006] Purpose of the invention: the present invention discloses a plating solution formula for preparing an electroless nickel-molybdenum-phosphorus alloy solution for preparing high molybdenum and high phosphorus coatings, so as to solve the problem that the current electroless nickel-molybdenum-phosphorus plating solution cannot prepare Mo and P content at the same time The problem of higher plating
Method used
the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more
Image
Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
Click on the blue label to locate the original text in one second.
Reading with bidirectional positioning of images and text.
Smart Image
Examples
Experimental program
Comparison scheme
Effect test
Embodiment 1
[0061] Nickel sulfate: 26 g / L
[0062] Sodium hypophosphite: 27 g / l
[0063] Sodium molybdate: 0.6 g / L
[0064] Sodium citrate: 40 g / l
[0065] Propionic acid: 1ml / L
[0066] Sodium tetraborate: 10 g / L
[0067] Sodium acetate: 10 g / L
[0068] Saccharin: 0.8 g / L
[0069] pH: 8.5 (adjust pH with ammonia water)
[0070] Temperature: 80°C
[0071] Add water to volume
Embodiment 2
[0073] Nickel sulfate: 36 g / L
[0074] Sodium hypophosphite: 37 g / l
[0075] Sodium molybdate: 0.7 g / L
[0076] Sodium citrate: 50 g / l
[0077] Propionic acid: 2.5 ml / l
[0078] Sodium tetraborate: 15 g / L
[0079] Sodium acetate: 20 g / l
[0080] Saccharin: 0.9 g / l
[0081] pH: 8.5 (adjust pH with ammonia water)
[0082] Temperature: 80°C
[0083] Add water to volume
Embodiment 3
[0085] Nickel sulfate: 30 g / L
[0086] Sodium hypophosphite: 32 g / L
[0087] Sodium molybdate: 0.66 g / L
[0088] Sodium citrate: 45 g / l
[0089] Propionic acid: 2ml / L
[0090] Sodium tetraborate: 12 g / l
[0091] Sodium acetate: 15 g / l
[0092] Saccharin: 0.84 g / L
[0093] pH: 8.3 (adjust pH with ammonia water)
[0094] Temperature: 76°C
[0095] Add water to volume
the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more
PUM
Login to view more
Abstract
The invention discloses a chemical nickel-plating-molybdenum-phosphorus alloy solution for preparing a high molybdenum and high phosphorus coating. The problem that an existing chemical nickel-plating-molybdenum-phosphorus alloy solution cannot simultaneously prepare a coating with high Mo and P contents is solved. The chemical nickel-plating-molybdenum-phosphorus alloy solution comprises nickel sulfate, sodium hypophosphite, sodium molybdate, sodium citrate, propionic acid, sodium tetraborate, sodium acetate and saccharin; and the PH is 8.0-8.5, and the plating solution temperature is 75-80 DEG C. The deposition rate of the coating is required to be controlled at 5-8 microns per hour. The results of scanning electron microscopy showed that the contents of molybdenum and phosphorus are higher in the coating prepared by the chemical nickel-plating-molybdenum-phosphorus alloy solution. The chemical nickel-plating-molybdenum-phosphorus alloy solution can be widely used in the field whichboth the thermal stability and amorphous structures are required and a chemical nickel-plating-molybdenum-phosphorus coating is used as a diffusion impervious layer in electron industries.
Description
technical field [0001] The invention relates to nickel-molybdenum-phosphorus ternary alloy electroless plating in the field of material surface treatment, especially in the field of the electronic industry that requires both thermal stability and amorphous structure as a diffusion barrier layer. Background technique [0002] The ternary alloy nickel-molybdenum-phosphorus coating is more excellent than the binary alloy nickel-phosphorus coating. At present, in the field of copper interconnection of integrated circuits, nickel-molybdenum-phosphorus coating can be used as a diffusion barrier layer in the field of copper interconnection of integrated circuits to prevent copper Diffusion into silicon dioxide is very important to improve the reliability of silicon-based integrated circuits. [0003] The electroless plating ternary alloy nickel-molybdenum-phosphorus process is developed on the basis of the electroless plating binary alloy nickel-phosphorus. The introduction of met...
Claims
the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more
Application Information
Patent Timeline
Application Date:The date an application was filed.
Publication Date:The date a patent or application was officially published.
First Publication Date:The earliest publication date of a patent with the same application number.
Issue Date:Publication date of the patent grant document.
PCT Entry Date:The Entry date of PCT National Phase.
Estimated Expiry Date:The statutory expiry date of a patent right according to the Patent Law, and it is the longest term of protection that the patent right can achieve without the termination of the patent right due to other reasons(Term extension factor has been taken into account ).
Invalid Date:Actual expiry date is based on effective date or publication date of legal transaction data of invalid patent.
Login to view more 
Login to view more