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38results about How to "High molybdenum content" patented technology

High-performance cold extrusion die steel and metallurgical manufacturing method thereof

ActiveCN101649419AReduced brittle tendencyImprove metallurgical qualitySteelmakingChemical composition
The invention provides high-performance cold extrusion die steel and metallurgical manufacturing method thereof. The high-performance cold extrusion die steel comprises the following chemical components in percentage by mass: 0.95 to 1.02 percent of C, 0.20 to 0.40 percent of Mn, 8.60 to 9.00 percent of Cr, 0.87 to 1.10 percent of Si, 1.80 to 2.00 percent of Mo, 0.40 to 0.60 percent of V, less than or equal to 0.30 percent of Cu, less than or equal to 0.25 percent of Ni, less than or equal to 0.025 percent of P, less than or equal to 0.010 percent of S, and the balance of Fe and inevitable impurities. According to the component proportion, the toughness performance of the high-performance cold extrusion die steel can be greatly improved. The metallurgical manufacturing method comprises theprocesses of electric furnace steel making, electroslag remelting and steel forging by a radial forging press. In the process of electroslag remelting, the voltage is between 57 and 59V, and the current is between11,000 and 12,000A; and in the process of steel forging by the radial forging press, steel ingots are heated to between 1,150 DEG C and 1,170 DEG C, and the temperature keeps for 2 to 4hours. The method is simple and convenient, and can remarkably improve the performance index of the steel.
Owner:宝武特种冶金有限公司

Molybdenum modification dispersant, and preparation method and applications thereof

The invention discloses a molybdenum modification dispersant, and a preparation method and applications thereof. The molybdenum modification dispersant comprises an imine diethanol molybdic acid diester group. The preparation method comprises the following steps: mixing succinic acid with alkyl chains and / or succinic anhydride with alkyl chains, alcohol amine compounds, and / or a diluent, carrying out first-phase reactions, removing residual unreacted substances that may exist, and adding a molybdenum reagent to carry out second phase reactions to obtain the target product. The molybdenum modification dispersant does not contain any sulfur or phosphor. Each molecule comprises an imine diethanol molybdic acid diester group, and thus the molybdenum content of the dispersant can be increased. Moreover, the raw material namely succinic acid with alkyl chains is commercial, the cost is largely reduced; the dispersant can generate a prominent high temperature synergetic antioxidant effect with alkylated diphenylamine antioxidant in lubricating oil; moreover, the dispersant can generate a good synergetic wear-resistant and friction reducing effect with zinc dialkyl dithiophosphate, the using amount of similar additive is reduced, the phosphor content is reduced, and the economy of fuel oil is improved.
Owner:江西福安路润滑材料有限公司

Preparation method of molybdenum-sulfur complex lubricating oil additive with high molybdenum content

The invention discloses a preparation method of a molybdenum-sulfur complex lubricating oil additive with high molybdenum content. The preparation method comprises the following steps: I, preparing a mixed liquid A from a hexavalent molybdenum compound, a sulfur-containing compound and distilled water, and then adjusting a pH value; II, adding dialkyl amine into the mixed liquid A which is subjected to pH value adjustment, then stirring, and then adding a phase transfer catalyst to obtain a mixed liquid B; III, under the protection of a nitrogen atmosphere, dropwise adding carbon disulfide into the mixed liquid B to obtain a mixed liquid C; and IV, standing the mixed liquid C till the mixed liquid C is layered, removing a water phase, washing an organic phase by virtue of an alkaline solution and an organic solvent, then distilling, and drying to obtain the high-molybdenum-content molybdenum-sulfur complex lubricating oil additive of which the mass percentage content of molybdenum is not less than 10%. The preparation method disclosed by the invention is simple in preparation process, and is favorable for industrial production; and the prepared molybdenum-sulfur complex lubricating oil additive has relatively high molybdenum content and good oil solubility, and after the additive is added into lubricating oil, the anti-wear and friction reduction properties of the lubricating oil can be greatly improved.
Owner:NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH

Method for preparing high-purity molybdenum trioxide from molybdenum concentrate through hydrometallurgy

The invention provides a method for preparing high-purity molybdenum trioxide from molybdenum concentrate through hydrometallurgy. The method comprises steps as follows: the molybdenum concentrate anddeionized water are mixed uniformly, and molybdenum concentrate pulp is prepared; the molybdenum concentrate pulp is subjected to a high-pressure oxygenolysis reaction, the reacted pulp is filtered;an obtained filter cake is subjected to alkaline leaching, filtered and washed, and a molybdate solution and waste residues are obtained; obtained filtrate and the molybdate solution are mixed, alkaliis added to adjust the pH, and the mixture is precipitated for impurity removal; the pH of a solution obtained after filtration of precipitates is adjusted to be neutral, a precipitation aid is addedand mixed sufficiently, and sulfuric acid is continuously added for pH adjustment, and acid settlement is performed; a material subjected to acid settlement is filtered again, a filter cake is calcined, and the high-purity molybdenum trioxide is obtained. The molybdenum content of the high-purity molybdenum trioxide obtained with the method can reach 66% or above, the total recovery rate of molybdenum can reach 98% or above, and meanwhile, raw gypsum products can be produced. The method is a production process which cannot cause environmental pollution, adopts a simple technological process and is used for preparing the high-purity molybdenum trioxide.
Owner:HENAN UNIV OF SCI & TECH

Foamed nickel-molybdenum alloy doped with carbon quantum dots and preparation method

The invention discloses a carbon quantum dot-doped foamed nickel-molybdenum alloy and a preparation method thereof. The method comprises the following steps: (1) preparing a part of electroplate liquid for electrodeposition of the foamed nickel-molybdenum alloy according to a known formula; (2) preparing a glucose carbon quantum dot solution by adopting a glucose hydrothermal method; (3) freezing and drying glucose carbon quantum dots into a carbon quantum dot solid, grinding the carbon quantum dot solid into carbon quantum dot powder, and adding the carbon quantum dot powder into the solution obtained in the step (1) to obtain an electro-deposition solution; (4) using nickel and molybdenum as anodes, foamed nickel as a cathode, placing the anodes and the cathodes in the electro-deposition solution, and performing electro-deposition in a single-cathode and double-anode mode; and (5) heating the solution to 35-55 DEG C, and carrying out electro-deposition under the condition that the apparent cathode current density is 110-130 mA/cm<2>. The foamed nickel-molybdenum alloy doped with the carbon quantum dots prepared by the method has the beneficial effects of good plating quality, good hydrogen evolution effect, high stability and high molybdenum content.
Owner:HUNAN UNIV

Cultivation method for molybdenum-enriched corn

The invention discloses a cultivation method for molybdenum-enriched corn, and belongs to the technical field of crop planting. The cultivation method for the molybdenum-enriched corn includes conventional steps of land selection and preparation, seed selecting, soaking and sowing, fertilization, field management and harvesting. In the seed soaking step, plump corn seeds free from disease and pest injuries are soaked in a molybdenum-enriched solution for 3-8 hours; fertilizer applied in the fertilization step refers to molybdenum fertilizer and compound fertilizer; according to the field management step, in the corn earing stage, a molybdenum-enriched nutrient solution is sprayed onto corn plants, and the molybdenum fertilizer is applied additionally. The molybdenum-enriched nutrient solution and the molybdenum fertilizer contain rich molybdenum, and accordingly, absorption of the corn plants is benefited; through seed soaking by the molybdenum-enriched nutrient solution and application of the molybdenum fertilizer, the content of molybdenum in the corn plants is increased effectively; through spraying of the molybdenum-enriched nutrient solution and additional application of the molybdenum fertilizer to the corn plants in the corn earing stage, the corn plants can absorb the microelement molybdenum better, growth of the corn plants is promoted, and yield and nutrition ingredients of the corn are increased.
Owner:陈国仁

A hydrogenation catalyst and its preparation method and use method

The invention discloses a hydrogenation catalyst, a preparation method and an application method thereof. It uses organic phosphonic acid and molybdenum source as reaction raw materials, utilizes the reaction of the two, and bonds the two together to prepare a hydrogenation catalyst. Among them, the inventors found for the first time that P in the organic phosphonic acid can change the surface acidity of the active phase, increase the surface acidity of the hydrogenation catalyst after sulfidation, and the increase in acidity helps to enhance the hydrogenation activity of the hydrogenation catalyst; in addition, the presence of P has It helps stabilize asphaltenes, thereby inhibiting asphaltene condensation and coking, thereby reducing the amount of coke, slowing down catalyst deactivation, and finally reducing the coking rate and increasing the hydrogenation yield. At the same time, it is also found that the presence of P helps to change the structure of the active phase in the hydrogenation catalyst, which can reduce the amount of molybdenum with a tetrahedral structure that is difficult to vulcanize, and increase the amount of molybdenum with an octahedral structure that is easy to sulfide, which in turn facilitates the sulfuration of molybdenum. In the process, it is converted into molybdenum disulfide with suitable stacking layers, thereby increasing the activity of the hydrogenation catalyst and increasing the hydrogenation yield.
Owner:FUZHOU UNIV

Preparation method of organic three-nuclear molybdenum additive

The invention discloses a preparation method of an organic three-nuclear molybdenum additive. The preparation method comprises the following steps: firstly, preparing tetralkyl disulfide thiuram by adopting dialkyl secondary amine, carbon disulphide, ethanol aqueous solution of sodium hydroxide and hydrogen peroxide; secondly, preparing a crude organic three-nuclear molybdenum additive by adoptingammonium trithio molybdate crystals, the tetralkyl disulfide thiuram and a mixed solvent; thirdly, performing post-treatment on the crude organic three-nuclear molybdenum additive to obtain an oily organic three-nuclear molybdenum additive. The invention creatively designs the preparation method of the organic three-nuclear molybdenum additive; the organic three-nuclear molybdenum additive is synthesized by adopting the ammonium trithio molybdate crystals and the tetralkyl disulfide thiuram; compared with the existing two-nuclear molybdenum additive, the molybdenum content is higher; under the same friction performance, the adding amount of the additive added into lubricating oil is smaller, and the friction resistance is more excellent; toxic and harmful raw materials are not used in a preparation process, the emission of the toxic and harmful gas is also avoided, and the method is green and environment-friendly.
Owner:NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH
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