Scale inhibitor, and preparation method thereof
A technology of scale inhibitor and catalyst, which is applied in the field of scale inhibitor preparation, can solve the problems of high preparation process requirements and high production cost, unsatisfactory scale inhibition effect of scale inhibitor, and given biodegradability of scale inhibitor, etc., to achieve Improve degradation performance and scale inhibition performance, excellent biodegradation performance, good inhibition effect
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Embodiment 1
[0040] Under nitrogen protection, 20g itaconic acid and 10g maleic anhydride are dissolved in 60g deionized water to be mixed with monomer A solution, add chain transfer agent 6g isopropanol and catalyzer 0.03g ferric sulfate in above-mentioned monomer A solution, regulate Temperature to 70°C, stirred for 10 minutes, and prepared as a mixed solution; weighed 12g of potassium persulfate dissolved in 27g of deionized water to prepare an oxidizing agent solution, weighed 8g of sodium sulfite dissolved in 27g of deionized water to prepare a reducing agent solution, weighed 10g respectively Acrylic acid, 10g methyl acrylate, and 10g vinyl acetate are mixed as monomer B, and the oxidant solution, reducing agent solution and monomer B are added dropwise to the above mixed solution at the same time within 3 hours (hrs), and the temperature is adjusted to 80 ° C for 6 hrs , cooled to room temperature to obtain antiscalant samples. When the dosage of the obtained scale inhibitor is 5ppm...
Embodiment 2
[0042] Under nitrogen protection, 15g itaconic acid and 15g maleic anhydride are dissolved in 60g deionized water and are mixed with monomer A solution, add chain transfer agent 6g isopropanol and catalyzer 0.03g ferric sulfate in above-mentioned monomer A solution, regulate Temperature to 70°C, stirred for 10 minutes, and prepared as a mixed solution; weighed 12g of potassium persulfate dissolved in 27g of deionized water to prepare an oxidizing agent solution, weighed 8g of sodium sulfite dissolved in 27g of deionized water to prepare a reducing agent solution, weighed 10g respectively Mix acrylic acid, 10g methyl acrylate, and 10g vinyl acetate as monomer B, add the oxidizing agent solution, reducing agent solution and monomer B to the above mixed solution dropwise within 3hrs, adjust the temperature to 80°C for 6hrs, and cool to room temperature Obtain antiscalant samples. When the dosage of the obtained scale inhibitor is 5ppm, the scale inhibition rate to calcium carbona...
Embodiment 3
[0044] Under nitrogen protection, 10g itaconic acid and 20g maleic anhydride are dissolved in 60g deionized water to be mixed with monomer A solution, add chain transfer agent 6g isopropanol and catalyst 0.03g ferric sulfate in above-mentioned monomer A solution, regulate Temperature to 70°C, stirred for 10 minutes, and prepared a mixed solution; weighed 12g potassium persulfate dissolved in 27g deionized water to prepare an oxidizing agent solution, weighed 8g sodium sulfite dissolved in 27g deionized water to prepare a reducing agent solution, weighed 10g respectively Mix acrylic acid, 10g methyl acrylate, and 10g vinyl acetate as monomer B, add the oxidizing agent solution, reducing agent solution and monomer B to the above mixed solution dropwise within 3hrs, adjust the temperature to 80°C for 6hrs, and cool to room temperature Obtain antiscalant samples. When the dosage of the obtained scale inhibitor is 5ppm, the scale inhibition rate to calcium carbonate is 62.1%; when ...
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