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Elastic sand-carrying fracturing fluid, thickener for the fracturing fluid and preparation method thereof

A thickening agent and fracturing fluid technology, applied in chemical instruments and methods, drilling compositions, etc., can solve problems such as large demand for surfactants, high requirements for construction equipment, and unfavorable environmental protection, and achieve construction results. The effect of obvious, low equipment requirements and fast dissolution rate

Active Publication Date: 2021-05-04
四川申和新材料科技有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although the viscoelastic surfactant cleaning fracturing fluid described in patent CN106268496A has good temperature resistance and simple process, the viscosity of the base fluid and the viscosity after cross-linking are high, the pumping of equipment is difficult, and the requirements for construction equipment are high. Sulfonic acid group, this group has great environmental pollution; the viscoelastic surfactant fracturing fluid described in patent CN103865511A is not resistant to temperature, is sensitive to temperature, the demand for surfactant is large, and the cost is expensive. The production cost of dialkylphthalein chloride is high, and the production process produces toxic hydrogen chloride gas, which is not conducive to environmental protection

Method used

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  • Elastic sand-carrying fracturing fluid, thickener for the fracturing fluid and preparation method thereof
  • Elastic sand-carrying fracturing fluid, thickener for the fracturing fluid and preparation method thereof
  • Elastic sand-carrying fracturing fluid, thickener for the fracturing fluid and preparation method thereof

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preparation example Construction

[0044] Its concrete preparation method is as follows:

[0045] 1. Preparation of thickener for elastic sand-carrying fracturing fluid

[0046] Dissolve analytically pure acrylamide in water, add octadecyltrimethylammonium bromide, potassium persulfate, and caustic soda under stirring, heat to 70°C, and then slowly add diethylene glycol distearate in sequence , tripolyglycerol diisostearate, sodium tetradecyl carboxylate, fatty acid amidopropyl dimethylamine, tertiary amino alcohol, fully reacted for 2 hours, passed nitrogen gas at 80°C to remove excess bromine to stop the reaction, and The obtained product is continuously passed through nitrogen to crystallize, and the crystallized product is dried and granulated to obtain the thickener.

[0047] 2. Preparation of elastic sand-carrying fracturing fluid

[0048] The preparation method in the laboratory of the elastic sand-carrying fracturing fluid provided by the invention is as follows:

[0049] In the laboratory, add water...

Embodiment 1

[0053] A thickener for elastic sand-carrying fracturing fluid, the preparation raw materials of the thickener include the following components in parts by weight: 0.5 part of acrylamide; 1 part of octadecyltrimethylammonium bromide; 0.05 parts of potassium persulfate; 0.005 parts of alkali; 1 part of diethylene glycol distearate; 0.5 parts of tripolyglycerol diisostearate; 0.2 parts of sodium tetradecyl carboxylate; 0.2 parts of amines; 0.2 parts of tertiary amino alcohols.

[0054] A preparation method for a thickener for elastic sand-carrying fracturing fluid, comprising the steps of:

[0055] A. Dissolve acrylamide in water to obtain an acrylamide solution:

[0056] B. In a stirring state, add octadecyltrimethylammonium bromide, potassium persulfate and caustic soda to the acrylamide solution and mix well to obtain an intermediate solution;

[0057] C. Add diethylene glycol distearate, triglyceryl diisostearate, sodium tetradecyl carboxylate, fatty acid amidopropyl dimeth...

Embodiment 2

[0062] A thickener for elastic sand-carrying fracturing fluid, the preparation raw materials of the thickener include the following components in parts by weight: 1.5 parts of acrylamide; 5 parts of octadecyltrimethylammonium bromide; 0.15 parts of potassium persulfate; 0.015 parts of alkali; 5 parts of diethylene glycol distearate; 1.5 parts of tripolyglycerol diisostearate; 0.8 parts of sodium tetradecyl carboxylate; 1.5 parts of amine; 0.8 parts of tertiary amino alcohol.

[0063] A preparation method for a thickener for elastic sand-carrying fracturing fluid, comprising the steps of:

[0064] A. Dissolve acrylamide in water to obtain an acrylamide solution:

[0065] B. In a stirring state, add octadecyltrimethylammonium bromide, potassium persulfate and caustic soda to the acrylamide solution and mix well to obtain an intermediate solution;

[0066] C. Add diethylene glycol distearate, triglyceryl diisostearate, sodium tetradecyl carboxylate, fatty acid amidopropyl dimet...

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Abstract

The invention belongs to the technical field of oilfield chemistry and fracturing stimulation, and provides an elastic sand-carrying fracturing fluid, a thickener used in the fracturing fluid and a preparation method thereof. The raw materials for the preparation of the thickener include the following parts by weight Number of components: 0.5-1.5 parts of acrylamide; 1-5 parts of octadecyltrimethylammonium bromide; 0.05-0.15 parts of potassium persulfate; 0.005-0.015 parts of alkali; diethylene glycol distearate 1-5 parts; 0.5-1.5 parts of tripolyglycerol diisostearate; 0.2-0.8 parts of sodium tetradecyl carboxylate; 0.2-1.5 parts of fatty acid amidopropyl dimethylamine; 0.2-0.8 parts of tertiary amino alcohol The elastic sand-carrying fracturing fluid is composed of the following components in weight percentage: thickener 0.20%-0.55%; crosslinking agent 0.20%-0.55%; drainage aid 0.1%-0.5%; anti-swelling agent 0.1% -0.5%; the balance is water; the preparation method includes the steps of preparing an acrylamide solution, an intermediate solution, a product, and a thickener. The elastic sand-carrying fracturing fluid of the present invention has simple liquid preparation, obvious construction effect and good rheological performance; after the thickener and cross-linking agent are used in combination, the viscosity is low and the sand-carrying ability is strong.

Description

technical field [0001] The invention belongs to the technical field of oilfield chemistry and fracturing stimulation, and in particular relates to an elastic sand-carrying fracturing fluid, a thickener used in the fracturing fluid and a preparation method thereof. Background technique [0002] At present, the prior art closest to the patent of the present invention is a gemini amphoteric viscoelastic surfactant and its preparation method and a clean fracturing fluid (patent number: CN106268496A) and viscoelastic surfactant using it as a thickening agent Fracturing fluid and its preparation method and application (patent number: CN103865511A). Although the viscoelastic surfactant cleaning fracturing fluid described in patent CN106268496A has good temperature resistance and simple process, the viscosity of the base fluid and the viscosity after cross-linking are high, the pumping of equipment is difficult, and the requirements for construction equipment are high. Sulfonic aci...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K8/68
CPCC09K8/685C09K8/882C09K8/887
Inventor 王愉屈川秦鹏
Owner 四川申和新材料科技有限公司
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