Heat-insulating nano-paint and preparation method thereof
A technology of nano-insulation and heat-insulating fillers, applied in fire-resistant coatings, epoxy resin coatings, reflective/signal coatings, etc., can solve problems such as poor high temperature resistance, paint peeling, and restrictions
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Embodiment 1
[0021] The preparation method of silicon nitride / epoxy resin is:
[0022] Add epoxy resin and silicon nitride to acetone, carry out ultrasonic dispersion to obtain a dispersion liquid, raise the temperature of the dispersion liquid to 78°C, then add vinyltrioxysilane, water and polyamide in sequence, stir evenly, and dry after the reaction That's it. The mass ratio of epoxy resin to silicon nitride is 6:1, the mass ratio of vinyltrioxysilane to epoxy resin is 1:25, and the mass ratio of polyamide to silicon nitride is 1:20.
Embodiment 2
[0024] The preparation method of silicon nitride / epoxy resin is:
[0025] Add epoxy resin and silicon nitride to acetone, carry out ultrasonic dispersion to obtain a dispersion liquid, raise the temperature of the dispersion liquid to 75-82°C, then add vinyltrioxysilane, water and polyamide in sequence, stir evenly, and the reaction ends Then dry it. The mass ratio of epoxy resin to silicon nitride is 8:1, the mass ratio of vinyltrioxysilane to epoxy resin is 1:15, and the mass ratio of polyamide to silicon nitride is 1:30.
Embodiment 3
[0027] A nano heat-insulating coating, calculated in parts by weight, comprises the following components:
[0028] 45 parts of acrylic emulsion, 30 parts of silicon nitride / epoxy resin, 15 parts of potassium hexatanate whiskers, 16 parts of silica airgel, 2 parts of ammonium acrylate dispersant, 0.8 parts of tetrachloroisophthalonitrile, 6 parts of modified ammonium polyacrylate, 2 parts of mineral oil, 9 parts of propylene glycol ether and 50 parts of deionized water.
[0029] Preparation:
[0030] 1) Add ammonium acrylate dispersant, tetrachloroisophthalonitrile, and 1 / 2 mineral oil into deionized water according to the formula amount, and stir and mix thoroughly at a speed of 300r / min;
[0031] 2) Add silica aerogel and potassium hexataftate whiskers to the mixture in step 1) and disperse at a rotating speed of 1000r / min;
[0032] 3) Add the mixture of acrylic emulsion and silicon nitride / epoxy resin, modified polyacrylic acid ammonium, propylene glycol ethyl ether and th...
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