Method for multi-level value-added utilization of camellia oleifera shells

A Camellia oleifera shell and multi-layered technology, applied in the field of resource utilization of food waste, can solve the problems of increasing solid waste pollution, waste of resources, etc.

Active Publication Date: 2018-10-30
江西绿野轩生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] In general research, the waste residue after extracting active substances is discarded or burned

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] The tea saponin, tannin-prebiotic-aromatic compound, high-quality food industry decolorizing activated carbon for poly-production of camellia oleifera husk includes the following process steps.

[0021] (1) Add 60-mesh camellia oleifera shell powder into acetone solution, ultrasonicate at 200W for 15 minutes, and then leaching for 5 minutes at a microwave power of 300W and a temperature of 60°C. The mass-volume ratio of the camellia oleifera shell to solvent is 1:10.

[0022] (2) Filter the reaction product of step (1) with filter paper, dry the remaining solid product at 105°C for 24 hours, add it to 70% ethanol solution, ultrasonicate at 200W for 15min, and treat it at 300W and 60°C for 5 minutes after ultrasonication. The mass volume ratio of the solid product to the solvent is 1:10.

[0023] (3) Filter the reaction product of step (2) with filter paper, dry the remaining solid product at 105°C for 24 hours, add 5% bran to supplement nutrients, inoculate edible fungi...

Embodiment 2

[0026] The tea saponin, tannin-prebiotic-aromatic compound, high-quality food industry decolorizing activated carbon for poly-production of camellia oleifera husk includes the following process steps.

[0027] (1) Add 60-mesh camellia oleifera shell powder into acetone solution, ultrasonicate at 100W for 30min, and then extract for 15min at a microwave power of 400W and a temperature of 50°C. The mass-volume ratio of the camellia oleifera shell to solvent is 1:20.

[0028] (2) Filter the reaction product of step (1) with filter paper, dry the remaining solid product at 105°C for 24 hours, add it to 70% ethanol solution, ultrasonicate at 100W for 30min, and treat it at 400W microwave power and 70°C for 15 minutes after ultrasonication. The mass volume ratio of the solid product to the solvent is 1:20.

[0029] (3) Filter the reaction product of step (2) with filter paper, dry the remaining solid product at 105°C for 24 hours, add 10% bran to supplement nutrients, inoculate edib...

Embodiment 3

[0032] The tea saponin, tannin-prebiotic-aromatic compound, high-quality food industry decolorizing activated carbon for poly-production of camellia oleifera husk includes the following process steps.

[0033] (1) Add 60-mesh camellia oleifera shell powder into acetone solution, ultrasonicate at 100W for 20min, and then leaching for 20min at a microwave power of 500W and a temperature of 40°C. The mass-volume ratio of the camellia oleifera shell to solvent is 1:30.

[0034] (2) Filter the reaction product of step (1) with filter paper, dry the remaining solid product at 105°C for 24 hours, add it to 70% ethanol solution, ultrasonicate at 100W for 20min, and treat it at 500W microwave power and 90°C for 20min after ultrasonication. The mass volume ratio of the solid product to the solvent is 1:30.

[0035] (3) Filter the reaction product of step (2) with filter paper, dry the remaining solid product at 105°C for 24 hours, add 15% bran to supplement nutrients, inoculate edible f...

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Abstract

The invention discloses a method for multi-level value-added utilization of camellia oleifera shells. The method comprises the following steps: firstly, crushing the camellia oleifera shells and screening by a 60-mesh sieve; obtaining tea saponins and tannins from the camellia oleifera shells by an ultrasonic-microwave synergistic stepwise extraction process; inoculating edible fungi after addinga small amount of brans into primary waste residues; raising the temperature and adding lysozyme to promote autolysis of edible fungal hyphae after the fungi grow all over a substrate; releasing cellulase and hemicellulase to obtain prebiotics rich in oligomeric cellulosic polysaccharide, oligomeric pentose and peptidoglycan; preparing secondary camellia oleifera shell waste residues with a high lignin content into an aromatic compound by a low-temperature microwave catalysis rapid-cracking technology; using the aromatic compound after separation and purification as a precursor for producing edible essence; and using residual biochar after steam activation for activated carbon for food industry. The method provided by the invention combines three major industries of edible camellia oleifera oil processing, food additive and biomass refining, proposes a new process of multi-level value-added utilization of the camellia oleifera shells, and can finally realize a new way of efficient value-added utilization of camellia oleifera shell resources without wastes in a whole process.

Description

technical field [0001] The invention belongs to the technical field of resource utilization of food waste, and relates to a method for preparing tea saponin, tannin, prebiotics, aromatic compounds and activated carbon for food industry decolorization through camellia oleifera shells. Background technique [0002] Camellia oleifera is an important woody oil crop in my country. It can produce 5.6 million tons of camellia oleifera fruit per year. As a by-product of camellia oil refinery, the annual output of camellia oleifera shell is as high as 3 million tons. It has not been effectively used as a by-product of agricultural processing for a long time. use. [0003] Tea saponin has various surface activities such as emulsification, dispersion, wetting, and foaming. It is an excellent natural phosphorus-free nonionic surfactant and is widely used in chemical, food, and pharmaceutical fields. Relevant studies have shown that the content of tea saponin in camellia oleifera husk ac...

Claims

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Application Information

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IPC IPC(8): B01D11/02C07H1/08C07H15/256C07J63/00C12P19/14
CPCB01D11/0265C07H1/08C07H15/256C07J63/00C12P19/14
Inventor 戴磊磊刘玉环王允圃阮榕生
Owner 江西绿野轩生物科技有限公司
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