Niclosamide ethanolamine dry flowable and preparation method thereof
The technology of spirulina ethanolamine salt and dry suspending agent is applied in the field of pesticides, which can solve the problems affecting the spray drying process and the high viscosity of the slurry, and achieve the effects of low storage and transportation cost, good dispersibility and good sieving performance.
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Embodiment 186
[0032] Embodiment 1 86% spiroxamine ethanolamine salt dry suspension concentrate
[0033] The formula is: 86% ethanolamine salt of spiroxamine, 3.2% hyperbranched polyamide ester as a dispersant, 1.6% fatty alcohol polyoxyethylene ether sulfate, 3.2% sodium lignosulfonate, and 1 sodium lauryl sulfate as a wetting agent %, sodium alkylnaphthalene sulfonate 2%, disintegrant ammonium sulfate 1%, diammonium hydrogen phosphate 1%, defoamer organosiloxane 0.5%, filler kaolin to make up 100%.
[0034] The preparation method is as follows:
[0035] 1. Mix the original medicine of spiroxamine ethanolamine salt, dispersant, wetting agent, disintegrant, defoamer, filler and water to obtain a slurry, and the amount of water is 45-50% of the total mass of each component.
[0036]2. Grind the uniformly mixed slurry with a sand mill until the particle size D90 is 3-5μm, then pump the suspoemulsion slurry into a pressure spray dryer for drying and granulation. The spray pressure is controlle...
Embodiment 2
[0037] Embodiment 2 80% dry suspension concentrate of spiroxamine ethanolamine salt
[0038] The formula is: spiroxamine ethanolamine salt 80%, dispersant hyperbranched polyamide ester 3.2%, fatty alcohol polyoxyethylene ether sulfate 1.6%, sodium lignosulfonate 3.2%, wetting agent sodium lauryl sulfate 1 %, sodium alkylnaphthalene sulfonate 2%, disintegrant ammonium sulfate 1%, diammonium hydrogen phosphate 1%, defoamer organosiloxane 0.5%, filler kaolin to make up 100%.
[0039] The preparation method is the same as in Example 1.
Embodiment 3
[0040] Example 3 70% spiroxamine ethanolamine salt dry suspension
[0041] The formula is: 70% ethanolamine salt of spiroxamine, 1.5% hyperbranched polyamide ester as a dispersant, 1.5% fatty alcohol polyoxyethylene ether sulfate, 3% sodium lignosulfonate, and 1.2% sodium lauryl sulfate as a wetting agent %, sodium alkylnaphthalene sulfonate 4.8%, disintegrant ammonium sulfate 1%, diammonium hydrogen phosphate 1%, defoamer organosiloxane 1%, filler kaolin supplement 100%.
[0042] The preparation method is the same as in Example 1.
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