Low temperature resistant environmentally-friendly sealant and preparation method thereof
An environment-friendly, low-temperature-resistant technology, applied in the field of sealants, can solve problems such as poor compatibility, poor low-temperature resistance, and reduced low-temperature resistance, and achieve the effects of improving bonding performance, improving low-temperature resistance, and increasing bonding strength
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Embodiment 1
[0033] A low-temperature resistant and environment-friendly sealant of this embodiment comprises the following raw materials in parts by weight:
[0034] 42 parts of blocked polydimethylsiloxane, 28 parts of modified epoxy resin, 14 parts of polytetrafluoroethylene, 16 parts of microsilica fume, 8 parts of crosslinking agent, 6 parts of adhesive, 5 parts of emperor felt moss , 6 parts of epoxidized soybean oil, 1 part of p-phenylenediamine, and 2 parts of ethylene glycol butyl ether.
[0035] The preparation method of the modified epoxy resin in this example is that the epoxy resin is added into the reaction kettle, the reaction temperature is 85°C, and the temperature is kept for 25 minutes, then the acidified graphene is added, ultrasonically dispersed, and dispersed for 6 minutes, and then polyurethane is added, and the reaction temperature Raise to 95°C, react for 35 minutes, then add polyisocyanate, continue to stir for 15 minutes, and then cool to room temperature to obt...
Embodiment 2
[0045] A low-temperature resistant and environment-friendly sealant of this embodiment comprises the following raw materials in parts by weight:
[0046] 46 parts of blocked polydimethylsiloxane, 32 parts of modified epoxy resin, 18 parts of polytetrafluoroethylene, 22 parts of microsilica fume, 14 parts of crosslinking agent, 10 parts of adhesive, 9 parts of imperial felt moss , 10 parts of epoxidized soybean oil, 3 parts of p-phenylenediamine, 6 parts of ethylene glycol butyl ether.
[0047] The preparation method of the modified epoxy resin in this embodiment is that the epoxy resin is added into the reaction kettle, the reaction temperature is 95° C., and the temperature is kept for 25-35 minutes, then acidified graphene is added, ultrasonically dispersed, dispersed for 10 minutes, and then polyurethane is added. The reaction temperature was raised to 105°C, reacted for 45 minutes, then added polyisocyanate, continued to stir for 25 minutes, and then cooled to room tempera...
Embodiment 3
[0057] A low-temperature resistant and environment-friendly sealant of this embodiment comprises the following raw materials in parts by weight:
[0058] 44 parts of end-blocked polydimethylsiloxane, 30 parts of modified epoxy resin, 16 parts of polytetrafluoroethylene, 19 parts of micro-silica fume, 11 parts of crosslinking agent, 8 parts of adhesive, 7 parts of emperor felt moss , 8 parts of epoxidized soybean oil, 2 parts of p-phenylenediamine, and 4 parts of ethylene glycol butyl ether.
[0059] The preparation method of the modified epoxy resin in this example is that the epoxy resin is added to the reaction kettle, the reaction temperature is 90°C, and the temperature is kept for 30 minutes, then acidified graphene is added, ultrasonically dispersed, dispersed for 8 minutes, and then polyurethane is added, and the reaction temperature Raise to 100°C, react for 40 minutes, then add polyisocyanate, continue to stir for 20 minutes, and then cool to room temperature to obtai...
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