Preparation method of membrane material capable of promoting denitrification and for pond culture
A membrane material and denitrification technology, applied in the field of preparation of membrane materials for pond culture, can solve problems such as application limitation, no bacteriostatic or bactericidal function, membrane biological fouling, etc., achieve good mechanical properties, improve load stability, reduce The effect of nitrogen content
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[0021] A method for preparing membrane materials for pond culture that promotes denitrification, comprising the following steps:
[0022] (1) Mix silicon dioxide, 2-(4-chlorosulfonic acid phenyl)ethyltrimethoxysilane and anhydrous toluene at a mass ratio of 3:1:36, heat up to 110°C, react for 20 hours, and then filter And wash 3 times with anhydrous toluene, vacuum dry at 70 ℃ for 10 hours for later use;
[0023] (2) Mix the product obtained in step 1 with ammonia water with a mass concentration of 15-25% at a mass ratio of 1:12, react at 40°C for 6 hours, filter after completion, and then mix with glacial acetic acid and sodium hypochlorite with a mass concentration of 8%. The solution was mixed at a mass ratio of 1.2:0.8:13 and reacted at 6°C for 90 minutes, then filtered, washed with water, and dried to obtain the product for use;
[0024] (3) Dissolve chitosan in isopropanol solution at a solid-to-liquid ratio of 1:16g / mL, then slowly add sodium hydroxide with a total mas...
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