Nano composite thermal-insulation paint and preparation method thereof
A thermal insulation coating and nano-composite technology, applied in the field of coatings, can solve problems such as poor high temperature resistance, coating peeling, and restricted application, and achieve the effect of reducing efficiency and improving dispersibility
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Embodiment 1
[0022] The preparation method of modified zirconia fiber comprises the following steps:
[0023] Add the zirconia fibers to dimethyl sulfoxide for ultrasonic dispersion to obtain a dispersion, then raise the temperature to 75°C, then add the silane coupling agent A-171 and silicon nitride, react for 12 hours, and then dry after the reaction. The mass ratio of zirconia fiber to silicon nitride is 3:1, and the mass ratio of zirconia fiber to silane coupling agent A-171 is 24:1.
Embodiment 2
[0025] The preparation method of modified zirconia fiber comprises the following steps:
[0026] Add the zirconia fiber to dimethyl sulfoxide for ultrasonic dispersion to obtain a dispersion liquid, then raise the temperature to 85°C, then add the silane coupling agent KH560 and silicon nitride, react for 6 hours, and then dry it after the reaction. The mass ratio of zirconia fiber to silicon nitride is 6:1, and the mass ratio of zirconia fiber to silane coupling agent KH560 is 18:1.
Embodiment 3
[0028] A nanocomposite thermal insulation coating, calculated in parts by weight, comprising the following components:
[0029] 30 parts of silicone resin emulsion, 8 parts of water-based fluorocarbon emulsion, 7 parts of nano-yttrium oxide, 12 parts of silica airgel, 8 parts of modified zirconia fiber of Example 1, 15 parts of nano-perlite, acrylate ammonium salt dispersant 2 parts, 2 parts of hydroxyethyl cellulose, 0.6 parts of polydimethylsiloxane solution and 20 parts of water.
[0030] Preparation method of nanocomposite thermal insulation coating:
[0031] 1) Add ammonium acrylate dispersant and 1 / 2 mass polydimethylsiloxane solution into dimethyl sulfoxide according to the formula amount, and stir and mix thoroughly at a speed of 500r / min;
[0032] 2) add silica airgel, the modified zirconia fiber of embodiment 1 and nano-perlite to the mixture of step 1) and disperse at a rotating speed of 1600r / min;
[0033] 3) Add silicone resin emulsion, aqueous fluorocarbon emul...
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