Image display device
An image display device, methyl technology, applied in adhesive types, film/sheet adhesives, instruments, etc., can solve the problems of reduced sensitivity and reduced operability of touch screens, and achieve excellent compressive strength, and Excellent peelability and high relative permittivity effect
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[0179] Hereinafter, the present invention will be described in more detail by showing examples, but the present invention is not limited thereto.
[0180] The physical properties of the copolymers obtained in the following production examples were measured by the following methods.
[0181] (Mw, Mw / Mn)
[0182] The weight average molecular weight and molecular weight distribution of the copolymer obtained in the following manufacture example were measured by gel permeation chromatography (GPC method) under the following conditions. ・Measuring device: HLC-8320GPC (manufactured by Tosoh Corporation)
[0183] ・The composition of the GPC column: the following 4 columns (all manufactured by Tosoh Co., Ltd.)
[0184] (1) TSKgel HxL-H (guard column)
[0185] (2) TSKgel GMHxL
[0186] (3) TSKgel GMHxL
[0187] (4)TSKgel G2500HxL
[0188] ·Flow rate: 1.0ml / min
[0189] ·Column temperature: 40℃
[0190] ·Sample concentration: 1.5% (w / v) (diluted with tetrahydrofuran)
[0191] ·M...
manufacture example A-1
[0196] In a four-necked flask with a capacity of 2 liters equipped with a stirrer, a thermometer, a nitrogen inlet pipe, and a cooling pipe, 14 parts by mass of n-butyl acrylate (BA), 20 parts by mass of methyl acrylate (MA), 60 parts by mass of 2-methoxyethyl acrylate and 6 parts by mass of acrylic acid (AA) were used as polymerizable monomers, and 150 parts by mass of ethyl acetate was added as a solvent.
[0197] Next, while stirring under a nitrogen atmosphere, 0.1 parts by mass of 2,2'-azobisisobutyronitrile (AIBN) was added as a polymerization initiator, and the reaction was carried out at 70°C for 7 hours. After completion of the reaction, the reaction solution was diluted with ethyl acetate to prepare a polymer solution containing the copolymer A-1 and having a solid content concentration of 20% by mass.
[0198] Mw of copolymer A-1 was 800,000, Mw / Mn was 3.0, and Tg was -34 degreeC.
manufacture example A-2
[0200] Except that the amount of n-butyl acrylate (BA) is changed from 14 parts by mass to 24 parts by mass, the amount of methyl acrylate (MA) is changed from 20 parts by mass to 30 parts by mass, and 2-methoxyethyl acrylate ( MEA) was changed from 60 parts by mass to 40 parts by mass, and reacted in the same manner as in Production Example A-1 to prepare a polymer solution containing copolymer A-2 with a solid content concentration of 20% by mass.
[0201] Mw of copolymer A-2 was 800,000, Mw / Mn was 2.5, and Tg was -29 degreeC.
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