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Method for extracting nutmeg oil

A technology of nutmeg oil and nutmeg, applied in the directions of essential oils/spice, fat production, etc., can solve the problems of insufficient nutmeg oil composition, lack of nutmeg characteristic taste, low product yield, etc. Oxidative deterioration, suitable for mass production, good quality effect

Inactive Publication Date: 2019-01-11
TIANJIN NAER BIOTECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The organic solvent extraction method uses n-hexane or ethanol as a solvent, heat reflux extraction method, the aromatic components are easy to degrade during the extraction, and the obtained essential oil also contains organic solvents, which affects the quality of the product
Moreover, there are many impurity components extracted by solvent method, such as resinous substances and waxy substances are extracted in large quantities, which seriously affects the quality of essential oils.
The composition of nutmeg oil obtained by steam distillation is not comprehensive enough, and some components cannot be extracted, resulting in the loss of the characteristic taste of nutmeg. At the same time, the yield of the product obtained by steam distillation is also low, about 6%.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] A method for extracting nutmeg oil, comprising the steps of:

[0027] (i) Nutmeg powder preparation

[0028] After washing the fresh nutmeg, dry it in the dark; add the dried eucalyptus leaves into a stirring ball mill, grind at a rotating speed of 300r / min, and sieve to obtain 20-mesh nutmeg powder;

[0029] (ii) Nutmeg powder pretreatment

[0030] Put the nutmeg powder in the extraction kettle, preheat the production equipment to 55°C, and pump the pressure in the extraction kettle and separation kettle to -0.1MPa;

[0031] (iii) Extraction

[0032] Inject the extraction agent butane into the extraction kettle for extraction to obtain an oil-soluble mixture. The liquid level of the extraction agent butane is completely submerged in the nutmeg powder. The extraction temperature is 55°C, the extraction pressure is 0.1 MPa, and the extraction time is 40 minutes;

[0033] (ⅳ) Precipitation and separation

[0034] The oil-soluble mixture is introduced into the separati...

Embodiment 2

[0042] A method for extracting nutmeg oil, comprising the steps of:

[0043] (i) Nutmeg powder preparation

[0044] Wash the fresh nutmeg and dry it in the dark; add the dried eucalyptus leaves into a stirring ball mill, grind at a speed of 500r / min, and sieve to obtain 40 mesh nutmeg powder;

[0045] (ii) Nutmeg powder pretreatment

[0046] Put the nutmeg powder in the extraction kettle, preheat the production equipment to 80°C, and pump the pressure inside the extraction kettle and separation kettle to -0.1MPa;

[0047] (iii) Extraction

[0048] Inject the extractant into the extraction kettle for extraction to obtain an oil-soluble mixture. The liquid level of the extractant is completely submerged in the nutmeg powder. The extraction temperature is 80°C, the extraction pressure is 1.0 MPa, and the extraction time is 60 minutes;

[0049] (ⅳ) Precipitation and separation

[0050] The oil-soluble mixture is introduced into the separation tank, and the oil-soluble mixture ...

Embodiment 3

[0058] A method for extracting nutmeg oil, comprising the steps of:

[0059] (i) Nutmeg powder preparation

[0060] After washing the fresh nutmeg, dry it in the dark; add the dried eucalyptus leaves into a stirring ball mill, grind at a speed of 400r / min, and sieve to obtain 30-mesh nutmeg powder;

[0061] (ii) Nutmeg powder pretreatment

[0062] Put the nutmeg powder in the extraction kettle, preheat the production equipment to 68°C, and pump the pressure in the extraction kettle and separation kettle to -0.1MPa;

[0063] (iii) Extraction

[0064] Inject butane into the extraction kettle for extraction to obtain an oil-soluble mixture. The butane liquid level completely submerges the nutmeg powder, the extraction temperature is 68°C, the extraction pressure is 0.5 MPa, and the extraction time is 50 minutes;

[0065] (ⅳ) Precipitation and separation

[0066] The oil-soluble mixture is introduced into the separation kettle, and the oil-soluble mixture is heated and depress...

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PUM

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Abstract

The invention provides a method for extracting nutmeg oil. The method comprises the following steps: (i) preparation of nutmeg powder; (ii) pretreatment of nutmeg powder; (iii) extraction; (iv) desolvation separation; (v) recovery of a liquid extractant; and (vi) residue collection. According to the invention, by using the unique dissolving property of the active ingredients of the nutmeg oil through the extractant, the nutmeg oil is extracted and separated, the recycling of a solvent is realized, and the utilization rate of the raw material can be increased; the extraction and separation process of the nutmeg oil can be completed under medium and low pressure conditions, the requirements for production equipment is reduced, safety performance of the production equipment is increased, andthe method is suitable for large scale production; the nutmeg has low cost, so that the production cost is obviously reduced. An extraction process is carried out under medium temperature conditions without destroying the active substance of the nutmeg oil, so that the flavor of the nutmeg can be completely preserved, the quality is good, and the oil yield is high, so that the problem of loss of the nutmeg oil and oxidative deterioration due to high temperature can be solved.

Description

technical field [0001] The invention belongs to a method for extracting natural vegetable oil, in particular to a method for extracting nutmeg oil. Background technique [0002] Nutmeg is the dry seed kernel of the nutmeg plant Nutmeg, warm in nature, pungent in taste, and returns to the spleen, stomach, and large intestine meridians. Warming middle-JIA and promoting qi, astringent intestines for relieving diarrhea. For spleen and stomach deficiency and cold, chronic diarrhea, abdominal distension and pain in the hospital, and vomiting due to lack of food. It is mainly produced in Malaysia, Indonesia, Sri Lanka and other countries. In addition, it is also produced in the West Indies. In addition, in the past, my country only cultivated nutmeg in Taiwan, Yunnan and other places. In recent years, it has been successfully introduced in a large area in Hainan, but most of the medicinal materials are imported. [0003] Nutmeg oil is a volatile oil extracted from nutmeg, which i...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/02
CPCC11B9/025
Inventor 孙静张荣飞李汝娟
Owner TIANJIN NAER BIOTECH
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