Method for extracting nutmeg oil
A technology of nutmeg oil and nutmeg, applied in the directions of essential oils/spice, fat production, etc., can solve the problems of insufficient nutmeg oil composition, lack of nutmeg characteristic taste, low product yield, etc. Oxidative deterioration, suitable for mass production, good quality effect
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Embodiment 1
[0026] A method for extracting nutmeg oil, comprising the steps of:
[0027] (i) Nutmeg powder preparation
[0028] After washing the fresh nutmeg, dry it in the dark; add the dried eucalyptus leaves into a stirring ball mill, grind at a rotating speed of 300r / min, and sieve to obtain 20-mesh nutmeg powder;
[0029] (ii) Nutmeg powder pretreatment
[0030] Put the nutmeg powder in the extraction kettle, preheat the production equipment to 55°C, and pump the pressure in the extraction kettle and separation kettle to -0.1MPa;
[0031] (iii) Extraction
[0032] Inject the extraction agent butane into the extraction kettle for extraction to obtain an oil-soluble mixture. The liquid level of the extraction agent butane is completely submerged in the nutmeg powder. The extraction temperature is 55°C, the extraction pressure is 0.1 MPa, and the extraction time is 40 minutes;
[0033] (ⅳ) Precipitation and separation
[0034] The oil-soluble mixture is introduced into the separati...
Embodiment 2
[0042] A method for extracting nutmeg oil, comprising the steps of:
[0043] (i) Nutmeg powder preparation
[0044] Wash the fresh nutmeg and dry it in the dark; add the dried eucalyptus leaves into a stirring ball mill, grind at a speed of 500r / min, and sieve to obtain 40 mesh nutmeg powder;
[0045] (ii) Nutmeg powder pretreatment
[0046] Put the nutmeg powder in the extraction kettle, preheat the production equipment to 80°C, and pump the pressure inside the extraction kettle and separation kettle to -0.1MPa;
[0047] (iii) Extraction
[0048] Inject the extractant into the extraction kettle for extraction to obtain an oil-soluble mixture. The liquid level of the extractant is completely submerged in the nutmeg powder. The extraction temperature is 80°C, the extraction pressure is 1.0 MPa, and the extraction time is 60 minutes;
[0049] (ⅳ) Precipitation and separation
[0050] The oil-soluble mixture is introduced into the separation tank, and the oil-soluble mixture ...
Embodiment 3
[0058] A method for extracting nutmeg oil, comprising the steps of:
[0059] (i) Nutmeg powder preparation
[0060] After washing the fresh nutmeg, dry it in the dark; add the dried eucalyptus leaves into a stirring ball mill, grind at a speed of 400r / min, and sieve to obtain 30-mesh nutmeg powder;
[0061] (ii) Nutmeg powder pretreatment
[0062] Put the nutmeg powder in the extraction kettle, preheat the production equipment to 68°C, and pump the pressure in the extraction kettle and separation kettle to -0.1MPa;
[0063] (iii) Extraction
[0064] Inject butane into the extraction kettle for extraction to obtain an oil-soluble mixture. The butane liquid level completely submerges the nutmeg powder, the extraction temperature is 68°C, the extraction pressure is 0.5 MPa, and the extraction time is 50 minutes;
[0065] (ⅳ) Precipitation and separation
[0066] The oil-soluble mixture is introduced into the separation kettle, and the oil-soluble mixture is heated and depress...
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