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Rapid detection kit of nitrite nitrogen, fabrication method of rapid detection kit and rapid detection method of nitrite nitrogen

A nitrite nitrogen and kit technology, which is applied in the direction of material analysis, measuring devices, instruments, etc. through observation of the influence on chemical indicators, can solve the problem of not providing an acidic buffer environment, the complicated operation process of the national standard method, and the reduction of stabilization time and other problems, to achieve the effect of low cost, stable detection reagents, and short stabilization time

Inactive Publication Date: 2019-01-15
SHENZHEN CHANGLONG TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] 2) The stabilization time is too long, which is 20 minutes, and the stabilization time needs to be appropriately reduced to achieve the purpose of rapid detection;
[0009] 4) The reaction of the national standard method needs to be carried out under strong acidic conditions, the pH cannot exceed 2, and the reaction system does not provide an appropriate acid buffer environment to cope with the complex water environment;
[0010] 5) The operation process of the national standard method is complicated, and a pipette is needed to pipette the solution, and a spectrophotometer is also used to measure the concentration, so it is urgent to simplify the process

Method used

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  • Rapid detection kit of nitrite nitrogen, fabrication method of rapid detection kit and rapid detection method of nitrite nitrogen

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preparation example Construction

[0053] see figure 1 , the present invention provides a kind of preparation method of nitrite nitrogen rapid detection kit, comprising the following steps:

[0054] Step 1, prepare the color-developing water agent, and use an opaque eye drop bottle to pack the color-developing water agent; wherein, the step of preparing the color-developing water agent includes: mixing deionized water with concentrated hydrochloric acid to obtain the color-developing water agent Color agent.

[0055] Specifically, the eye drops bottle is a liquid container that can control the amount of drops that are dropped out by pinching or squeezing.

[0056] Specifically, the step 1 includes: adding a certain volume of deionized water to the clean container, then mixing a certain volume of concentrated hydrochloric acid, and then quantitatively dispensing it into an opaque eye drops bottle;

[0057] Specifically, in the color developing water agent, the mass ratio of concentrated hydrochloric acid to de...

Embodiment 1

[0134] Monitoring of nitrite nitrogen in water samples of an aquaculture fish shop in Pingdi Street, Longgang District, Shenzhen—0.65mg / L NO 2 - -N.

[0135] 1. The preparation method of the nitrite nitrogen quick test kit includes:

[0136] 1) Preparation of color developing water agent:

[0137] Dissolve 10ml of concentrated hydrochloric acid into 90ml of deionized water, mix evenly, use 10ml opaque eye droppers to dispense the mixed solution, and store in a cool place away from light.

[0138] 2) Preparation of chromogenic powder:

[0139] Weigh 2g of p-aminobenzenesulfonamide, 0.1g of N-(1-naphthyl)-ethylenediamine dihydrochloride, 4g of sodium chloride, and 4g of citric acid monohydrate, and pour them into a mortar and mix well . Dry in a vacuum oven for 12 hours, then pack into aluminum foil bags, the weight of each bag of medicine is 0.08g, and the size of the aluminum foil bags is 3.5cm×3.5cm. Finally, the aluminum foil bag is sealed with a vacuum sealer.

[014...

Embodiment 2

[0147] Shenzhen Changlong Technology Co., Ltd. Biological total nitrogen removal project pilot test (the main body of the water sample is wastewater from a domestic sewage plant in Gaoming, Foshan, Guangdong). The concentration of nitrite nitrogen—2.71mg / L NO 2 - -N.

[0148] 1. The preparation method of the nitrite nitrogen quick test kit includes:

[0149] 1) Preparation of color developing water agent:

[0150] Dissolve 20ml of concentrated hydrochloric acid into 180ml of deionized water, mix evenly, use 10ml opaque eye droppers to dispense the mixed solution, and store in a cool place away from light.

[0151] 2) Preparation of chromogenic powder:

[0152] Take by weighing 2.4g p-aminobenzenesulfonamide, 0.12g N-(1-naphthyl)-ethylenediamine dihydrochloride, 4.8g sodium chloride, 4.8g citric acid monohydrate four kinds of medicines respectively, pour into Bowl to mix. Place in a vacuum drying oven to dry for 12 hours, and pack into aluminum foil bags. The weight of ea...

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Abstract

The invention discloses a rapid detection kit of nitrite nitrogen, a fabrication method of the rapid detection kit and a rapid detection method of the nitrite nitrogen. The rapid detection kit of thenitrite nitrogen comprises a package container, a developing water agent, a developing powder agent, a standard color card, an injector, a detection bottle and a second container, wherein the developing water agent, the developing powder agent, the standard color card, the injector, the detection bottle and the second container are accommodated in the package container, the detection bottle is provided with graduation lines, the second container is loaded with dilution water, the developing water agent and the developing powder agent are respectively loaded in a lightproof eyedrop bottle and alightproof first container, the developing water agent is diluted hydrochloric acid, and the developing powder agent is a mixed powder agent containing p-acetaminobenzenesulfamide, N-(1-naphthyl)-ethylenediamine dihydrochloride, sodium chloride, citric acid and / or a hydrate thereof. The rapid detection kit of the nitrite nitrogen is convenient to use, rapid detection of a site can be achieved, the rapid detection kit has relatively high practicability, and great convenience can be provided for a detection site in lack of detection equipment.

Description

technical field [0001] The invention relates to the field of water quality detection, in particular to a nitrite nitrogen rapid detection kit, a preparation method thereof and a nitrite nitrogen rapid detection method. Background technique [0002] Nitrite is an intermediate product of the nitrogen cycle and is unstable; it can be oxidized to nitrate or reduced to ammonia depending on the water environment conditions. Therefore, by measuring nitrite nitrogen (NO 2 - -N), and at the same time know the content of nitrate nitrogen and ammonia nitrogen in the water, you can judge whether the total amount of nitrogen compounds in the polluted water body exceeds the standard. Quantitative measures, such as using biochemical technology to control the content of nitrate nitrogen in sewage, and reducing the concentration of nitrate nitrogen through denitrification. If the denitrification process is not properly controlled, it will lead to the accumulation of nitrite nitrogen, whic...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/78
CPCG01N21/78G01N2021/775
Inventor 熊阳辉陈涛钦周小峰杨庆董林辉董红红范志伟朱芳芳蔡振山
Owner SHENZHEN CHANGLONG TECH CO LTD
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